Preparation of single high-Tc phase BiPbSrCaCuO superconductor by the EDTA precursor solution method

1991 ◽  
Vol 185-189 ◽  
pp. 513-514 ◽  
Author(s):  
C.Y. Shieh ◽  
Y. Huang ◽  
M.K. Wu ◽  
C.Y. Huang
Author(s):  
Shozo Ikeda ◽  
Hirotoshi Hayakawa ◽  
Daniel R. Dietderich

Pb addition makes easier to form the high Tc phase in the BSCCO system. However, Pb easily vaporized at high temperature. A controlled Pb potential method has been applied to grow the high Tc phase in films. Initially, films are deposited on cleaved MgO substrates using an rf magnetron sputtering system. These amorphous as-deposited films are heat treated in a sealed gold capsule along with a large pellet of Pb-added BSCCO. Details of the process and characterization of the films have been reported elsewhere (1). Films trated for 0.5h at 850° C contain mainly the low Tc phase with a small amount of the high Tc phase. Hawever, films treated for 3h at 850°C consist mainly of the high Tc phase. This film is superconductive with a Tc(zero) of 106K. The Pb/Bi ratio of the films, analysed by SEM- EDS, are 0.12 and 0.18 for heat tratment times of 0.5 and 3h, respectively. The present study investigates the modulated structures of these films using HREM.


2018 ◽  
Vol 31 (3) ◽  
pp. 26 ◽  
Author(s):  
Laheeb. A. Mohammed ◽  
Kareem. A. Jasim

   on this research is to study the effect of nickel oxide substitution on the pure phases superconductor Tl0.5Pb0.5Ba2Can-1Cun-xNixO2n+3-δ (n=3) where x=(0,0.2,0.4,0.6,0.8.and 1.0). The specimens in this work were prepared with used  procedure of solid state reaction with sintering temperature 8500C for 24 h .we used technical (4-prob)to calculated and the critical temperature Tc . The results of the XRD diffraction analysis showed that the structure for pure and doped phases was tetragonal with phases high-Tc phase (1223),(1212) and low-Tc phase (1202)  and add to the presence of some impure phase. It was noted the value a=b,c  the parameter of  the lattice increment  with the increment of Ni content. The increment of (NiO) concentration effects electrical resistivity, dielectric constant and the hardness.


1988 ◽  
Vol 35 (9) ◽  
pp. 1003-1009 ◽  
Author(s):  
Jun Takada ◽  
Hitoshi Kitaguchi ◽  
Kiichi Oda ◽  
Akiyoshi Osaka ◽  
Yoshinari Miura ◽  
...  
Keyword(s):  
High Tc ◽  

1990 ◽  
Vol 37 (1) ◽  
pp. 54-59 ◽  
Author(s):  
Jun Takada ◽  
Toshio Egi ◽  
Kiichi Oda ◽  
Hitoshi Kitaguchi ◽  
Akiyoshi Osaka ◽  
...  
Keyword(s):  
High Tc ◽  

1989 ◽  
Vol 36 (5) ◽  
pp. 527-532 ◽  
Author(s):  
Jun Takada ◽  
Kiichi Oda ◽  
Toshio Egi ◽  
Hitoshi Kitaguchi ◽  
Akiyoshi Osaka ◽  
...  

1992 ◽  
Vol 39 (5) ◽  
pp. 386-389
Author(s):  
Jun Takada ◽  
Masashi Fujiwara ◽  
Toshio Egi ◽  
Tokuro Nanba ◽  
Yasunori Ikeda ◽  
...  
Keyword(s):  
High Tc ◽  

1992 ◽  
Vol 39 (9) ◽  
pp. 783-786
Author(s):  
Naoya Kobayashi ◽  
Keiichi Morikawa ◽  
Masataka Kanai ◽  
Kazutoyo Shimizu ◽  
Yoshihiro Kusano ◽  
...  

2018 ◽  
Vol 554 ◽  
pp. 1-7 ◽  
Author(s):  
P. Neha ◽  
A. Bhardwaj ◽  
Vikrant Sahu ◽  
S. Patnaik

1992 ◽  
Vol 39 (9) ◽  
pp. 779-782 ◽  
Author(s):  
Jun Takada ◽  
Katsunori Hosotani ◽  
Masashi Fujiwara ◽  
Yoshihiro Kusano ◽  
Tokuro Nanba ◽  
...  

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