Modeling of reactive batch distillation processes for control

2019 ◽  
Vol 121 ◽  
pp. 86-98 ◽  
Author(s):  
Alejandro Marquez-Ruiz ◽  
Carlos S. Méndez-Blanco ◽  
Leyla Özkan
Keyword(s):  
Batch Distillation ◽  
Reactive Batch Distillation

Optimization Aspects for Reactive Batch Distillation.

2001 ◽  
Vol 34 (3) ◽  
pp. 312-318 ◽  
Author(s):  
SABINE GIESSLER ◽  
SHINJI HASEBE ◽  
IORI HASHIMOTO
Keyword(s):  
Batch Distillation ◽  
Reactive Batch Distillation

Dynamic modelling and simulation of reactive batch distillation

1999 ◽  
Vol 23 ◽  
pp. S423-S426 ◽  
Author(s):  
R. Schneider ◽  
C. Noeres ◽  
L.U. Kreul ◽  
A. Górak
Keyword(s):  
Dynamic Modelling ◽  
Modelling And Simulation ◽  
Batch Distillation ◽  
Reactive Batch Distillation

scholarly journals Control strategies for reactive batch distillation

1994 ◽  
Vol 4 (4) ◽  
pp. 205-217 ◽  
Author(s):  
Eva Sørensen ◽  
Sigurd Skogestad
Keyword(s):  
Control Strategies ◽  
Batch Distillation ◽  
Reactive Batch Distillation

Semi-Continuous Reactive Batch Distillation for Production of Methyl Formate

2011 ◽  
Vol 301-303 ◽  
pp. 290-297
Author(s):  
Ying Li ◽  
Hong Mei Qu ◽  
Ye Tian ◽  
Shuang Song ◽  
Peng Bai
Keyword(s):  
Formic Acid ◽  
Methyl Formate ◽  
Batch Reactor ◽  
Optimal Operation ◽  
Batch Distillation ◽  
Estimated Parameters ◽  
Runge Kutta Method ◽  
Different Temperatures ◽  
Reactive Batch Distillation ◽  
Kinetics Of

Reaction kinetics of the esterification of Methyl Formate (MF) is studied in a batch reactor at different temperatures and the reliability of the estimated parameters is analyzed with Matlab using a fourth order Runge-Kutta method in the paper. Kinetic constants were experimentally examined and used to calculate the optimal operation parameters of semi-continuous reactive distillation for production of MF in order to minimize the amount of unconverted Formic Acid (FA) remained in the bottom. The results show that the optimal condition is obtained at the formic acid/methanol mole ratio of 0.5:1 and the mass fraction of formic acid at the bottom is 2% which is very close to the calculated value. Simulation work was carried out with Matlab and the results showed good agreement with the experimental data.

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