Synthesis of nanocrystalline carbide in tungsten alloy by mechanical alloying and annealing

Formation of partial nanocrystal and amorphous tungsten alloys was synthesized via crystallization of a completely amorphized tungsten alloy synthesized by mechanical alloying. Structural characterization shows formation of amorphous structure from mechanical alloying of a mixture of elemental tungsten and iron powders after about 150 hours. Partial nanocrystalline phases within the amorphous matrix were formed through annealing the amorphous tungsten alloy at 1075°C.

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Microstructure of mechanically alloyed and hot-pressed Al5CuZr2

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100177982 ◽

1990 ◽

Vol 48 (4) ◽

pp. 970-971

Author(s):

T. E. Mitchell ◽

P. B. Desch ◽

R. B. Schwarz

Keyword(s):

Mechanical Alloying ◽

Vickers Hardness ◽

Hot Pressing ◽

Rapid Quenching ◽

Hardened Steel ◽

Alloyed Powder ◽

Ion Milling ◽

Mechanical Grinding ◽

Mechanically Alloyed ◽

Steel Container

Al3Zr has the highest melting temperature (1580°C) among the tri-aluminide intermetal1ics. When prepared by casting, Al3Zr forms in the tetragonal DO23 structure but by rapid quenching or by mechanical alloying (MA) it can also be prepared in the metastable cubic L12 structure. The L12 structure can be stabilized to at least 1300°C by the addition of copper and other elements. We report a TEM study of the microstructure of bulk Al5CuZr2 prepared by hot pressing mechanically alloyed powder.MA was performed in a Spex 800 mixer using a hardened steel container and balls and adding hexane as a surfactant. Between 1.4 and 2.4 wt.% of the hexane decomposed during MA and was incorporated into the alloy. The mechanically alloyed powders were degassed in vacuum at 900°C. They were compacted in a ram press at 900°C into fully dense samples having Vickers hardness of 1025. TEM specimens were prepared by mechanical grinding followed by ion milling at 120 K. TEM was performed on a Philips CM30 at 300kV.

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Dynamic Tensile Behavior of 93wt.% Tungsten Alloy and its Fractal Features of Fracture

Journal de Physique IV (Proceedings) ◽

10.1051/jp4:1997371 ◽

1997 ◽

Vol 07 (C3) ◽

pp. C3-409-C3-414

Author(s):

B.-P. Zhang ◽

C. Ding ◽

B. Liu ◽

T. Jiao ◽

H. Lin ◽

...

Keyword(s):

Tensile Behavior ◽

Tungsten Alloy

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Dynamic compaction domain (shock compaction energy vs. ρ0/ρ) for a Fe-15 atomic % Cu nanometric alloy obtained by mechanical alloying

Journal de Physique IV (Proceedings) ◽

10.1051/jp4:20020792 ◽

2003 ◽

Vol 110 ◽

pp. 803-808 ◽

Cited By ~ 1

Author(s):

R. G. Esquives ◽

E. M. Orozco ◽

C. T. Renero ◽

D. V. Jaramillo

Keyword(s):

Mechanical Alloying ◽

Dynamic Compaction ◽

Shock Compaction ◽

Compaction Energy

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Mechanical properties of FeAlSi powders prepared by mechanical alloying from different initial feedstock materials

Matériaux & Techniques ◽

10.1051/mattech/2018063 ◽

2019 ◽

Vol 107 (2) ◽

pp. 207 ◽

Cited By ~ 2

Author(s):

Jaroslav Čech ◽

Petr Haušild ◽

Miroslav Karlík ◽

Veronika Kadlecová ◽

Jiří Čapek ◽

...

Keyword(s):

Mechanical Properties ◽

Mechanical Alloying ◽

Young’S Modulus ◽

Milling Time ◽

Young's Modulus ◽

Element Model ◽

X Ray Diffraction ◽

X Ray ◽

Powder Particles ◽

Complete Homogenization

FeAl20Si20 (wt.%) powders prepared by mechanical alloying from different initial feedstock materials (Fe, Al, Si, FeAl27) were investigated in this study. Scanning electron microscopy, X-ray diffraction and nanoindentation techniques were used to analyze microstructure, phase composition and mechanical properties (hardness and Young’s modulus). Finite element model was developed to account for the decrease in measured values of mechanical properties of powder particles with increasing penetration depth caused by surrounding soft resin used for embedding powder particles. Progressive homogenization of the powders’ microstructure and an increase of hardness and Young’s modulus with milling time were observed and the time for complete homogenization was estimated.

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