High-pressure vertical Bridgman growth of lead magnesium niobate–lead titanate single crystal

2010 ◽  
Vol 312 (7) ◽  
pp. 971-977 ◽  
Author(s):  
Romit Dhar ◽  
Russell Tjossem ◽  
Kelvin G. Lynn
2004 ◽  
Vol 19 (2) ◽  
pp. 609-615 ◽  
Author(s):  
Raji Soundararajan ◽  
Rabindra Nath Das ◽  
Russ Tjossem ◽  
Amit Bandyopadhyay ◽  
Kelvin G. Lynn ◽  
...  

We have grown lead magnesium niobate–lead titanate (PMN–PT) single crystals, using the high-pressure vertical Bridgman (HPVB) technique, around the stoichiometric composition of 0.7 PMN–0.3PT [0.7Pb(Mg1/3Nb2/3)O3 + 0.3(PbTiO3)]. The final ingot (about 50-mm diameter, 25-mm long) was machinable using an inner diameter saw. The room-temperature x-ray diffraction on the starting powders and the final single crystal revealed a desirable perovskite structure. The natural growth direction in most of the crystals, as determined using orientation image microscopy, was (110). Examination of the final microstructures and phases/inclusions had been done using optical and infrared microscopy, energy dispersive spectroscopy, and x-ray backscatter techniques. Microstructural characterizations of the final ingots have revealed the presence of pores filled with Mg–Si–O-rich impurity phase, usually found along the cell boundary–like structures, in all the growths. We have measured some piezoelectric properties including d33 (1200 pC/N), k33 (0.85), kt (0.5), and the dielectric constant at the Curie temperature.


2003 ◽  
Vol 258 (3-4) ◽  
pp. 353-367 ◽  
Author(s):  
Kevin T Zawilski ◽  
M.Claudia C Custodio ◽  
Robert C DeMattei ◽  
Sang-Goo Lee ◽  
Ralph G Monteiro ◽  
...  

2013 ◽  
Vol 102 (4) ◽  
pp. 042906 ◽  
Author(s):  
Tian-Bing Xu ◽  
Laura Tolliver ◽  
Xiaoning Jiang ◽  
Ji Su

2012 ◽  
Vol 51 ◽  
pp. 07GE09 ◽  
Author(s):  
Daisuke Yamaguchi ◽  
Takefumi Kanda ◽  
Koichi Suzumori ◽  
Masataka Kuroda ◽  
Dai Takeda

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