scholarly journals Cryogenic Signal Amplification Combined with Helium-Temperature MAS DNP toward Ultimate NMR Sensitivity at High Field Conditions

2021 ◽  
pp. 107139
Author(s):  
Yoh Matsuki ◽  
Shinji Nakamura ◽  
Fumio Hobo ◽  
Yuki Endo ◽  
Hiroki Takahashi ◽  
...  
2014 ◽  
Vol 16 (45) ◽  
pp. 24672-24675 ◽  
Author(s):  
Andrey N. Pravdivtsev ◽  
Alexandra V. Yurkovskaya ◽  
Hans-Martin Vieth ◽  
Konstantin L. Ivanov

A new technique is proposed to carry out Signal Amplification By Reversible Exchange (SABRE) experiments at high magnetic fields.


2008 ◽  
Vol 29 (12) ◽  
pp. 1392-1394 ◽  
Author(s):  
SÉbastien Martinie ◽  
Daniela Munteanu ◽  
Gilles Le Carval ◽  
Jean-Luc Autran

1977 ◽  
Vol 83 (1) ◽  
pp. K87-K90 ◽  
Author(s):  
P. Novotný ◽  
V. Roskovec ◽  
J. Šternberk

Author(s):  
Maria Grazia Concilio ◽  
Ilya Kuprov ◽  
Lucio Frydman

Dynamic nuclear polarization (DNP) is widely used to enhance solid state nuclear magnetic resonance (NMR) sensitivity. Its efficiency as a generic signal-enhancing approach for liquid state NMR, however, decays rapidly...


2014 ◽  
Vol 86 (3) ◽  
pp. 1767-1774 ◽  
Author(s):  
Jan-Bernd Hövener ◽  
Niels Schwaderlapp ◽  
Robert Borowiak ◽  
Thomas Lickert ◽  
Simon B. Duckett ◽  
...  

Author(s):  
M.K. Lamvik ◽  
D.A. Kopf ◽  
S.D. Davilla ◽  
J.D. Robertson

Last year we reported1 that there is a striking reduction in the rate of mass loss when a specimen is observed at liquid helium temperature. It is important to determine whether liquid helium temperature is significantly better than liquid nitrogen temperature. This requires a good understanding of mass loss effects in cold stages around 100K.


Author(s):  
T. F. Kelly ◽  
P. J. Lee ◽  
E. E. Hellstrom ◽  
D. C. Larbalestier

Recently there has been much excitement over a new class of high Tc (>30 K) ceramic superconductors of the form A1-xBxCuO4-x, where A is a rare earth and B is from Group II. Unfortunately these materials have only been able to support small transport current densities 1-10 A/cm2. It is very desirable to increase these values by 2 to 3 orders of magnitude for useful high field applications. The reason for these small transport currents is as yet unknown. Evidence has, however, been presented for superconducting clusters on a 50-100 nm scale and on a 1-3 μm scale. We therefore planned a detailed TEM and STEM microanalysis study in order to see whether any evidence for the clusters could be seen.A La1.8Sr0.2Cu04 pellet was cut into 1 mm thick slices from which 3 mm discs were cut. The discs were subsequently mechanically ground to 100 μm total thickness and dimpled to 20 μm thickness at the center.


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