Three-dimensional high resolution X-ray imaging and quantification of lithium ion battery mesocarbon microbead anodes

2014 ◽  
Vol 248 ◽  
pp. 1014-1020 ◽  
Author(s):  
F. Tariq ◽  
V. Yufit ◽  
M. Kishimoto ◽  
P.R. Shearing ◽  
S. Menkin ◽  
...  
MRS Bulletin ◽  
1988 ◽  
Vol 13 (1) ◽  
pp. 13-18 ◽  
Author(s):  
J.H. Kinney ◽  
Q.C. Johnson ◽  
U. Bonse ◽  
M.C. Nichols ◽  
R.A. Saroyan ◽  
...  

Imaging is the cornerstone of materials characterization. Until the middle of the present century, visible light imaging provided much of the information about materials. Though visible light imaging still plays an extremely important role in characterization, relatively low spatial resolution and lack of chemical sensitivity and specificity limit its usefulness.The discovery of x-rays and electrons led to a major advance in imaging technology. X-ray diffraction and electron microscopy allowed us to characterize the atomic structure of materials. Many materials vital to our high technology economy and defense owe their existence to the understanding of materials structure brought about with these high-resolution methods.Electron microscopy is an essential tool for materials characterization. Unfortunately, electron imaging is always destructive due to the sample preparation that must be done prior to imaging. Furthermore, electron microscopy only provides information about the surface of a sample. Three dimensional information, of great interest in characterizing many new materials, can be obtained only by time consuming sectioning of an object.The development of intense synchrotron light sources in addition to the improvements in solid state imaging technology is revolutionizing materials characterization. High resolution x-ray imaging is a potentially valuable tool for materials characterization. The large depth of x-ray penetration, as well as the sensitivity of absorption crosssections to atomic chemistry, allows x-ray imaging to characterize the chemistry of internal structures in macroscopic objects with little sample preparation. X-ray imaging complements other imaging modalities, such as electron microscopy, in that it can be performed nondestructively on metals and insulators alike.


2008 ◽  
Vol 100 (5) ◽  
pp. 2966-2976 ◽  
Author(s):  
David D. Cox ◽  
Alexander M. Papanastassiou ◽  
Daniel Oreper ◽  
Benjamin B. Andken ◽  
James J. DiCarlo

Much of our knowledge of brain function has been gleaned from studies using microelectrodes to characterize the response properties of individual neurons in vivo. However, because it is difficult to accurately determine the location of a microelectrode tip within the brain, it is impossible to systematically map the fine three-dimensional spatial organization of many brain areas, especially in deep structures. Here, we present a practical method based on digital stereo microfocal X-ray imaging that makes it possible to estimate the three-dimensional position of each and every microelectrode recording site in “real time” during experimental sessions. We determined the system's ex vivo localization accuracy to be better than 50 μm, and we show how we have used this method to coregister hundreds of deep-brain microelectrode recordings in monkeys to a common frame of reference with median error of <150 μm. We further show how we can coregister those sites with magnetic resonance images (MRIs), allowing for comparison with anatomy, and laying the groundwork for more detailed electrophysiology/functional MRI comparison. Minimally, this method allows one to marry the single-cell specificity of microelectrode recording with the spatial mapping abilities of imaging techniques; furthermore, it has the potential of yielding fundamentally new kinds of high-resolution maps of brain function.


2016 ◽  
Vol 154 ◽  
pp. 27-33 ◽  
Author(s):  
Oluwadamilola O. Taiwo ◽  
Donal P. Finegan ◽  
Jeff Gelb ◽  
Christian Holzner ◽  
Daniel J.L. Brett ◽  
...  

2017 ◽  
Vol 3 (8) ◽  
pp. e1700971 ◽  
Author(s):  
Hasnain Hafiz ◽  
Kosuke Suzuki ◽  
Bernardo Barbiellini ◽  
Yuki Orikasa ◽  
Vincent Callewaert ◽  
...  

2019 ◽  
Vol 433 ◽  
pp. 126631 ◽  
Author(s):  
Christiane Rahe ◽  
Stephen T. Kelly ◽  
Mansoureh Nourozi Rad ◽  
Dirk Uwe Sauer ◽  
Joachim Mayer ◽  
...  

2018 ◽  
Author(s):  
Shuichiro Hirai ◽  
H. Naito ◽  
T. Yoshida ◽  
Takashi Sasabe ◽  
K. Kawamura ◽  
...  

Nanomaterials ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1721
Author(s):  
Heon Yong Jeong ◽  
Hyung San Lim ◽  
Ju Hyuk Lee ◽  
Jun Heo ◽  
Hyun Nam Kim ◽  
...  

The effect of scintillator particle size on high-resolution X-ray imaging was studied using zinc tungstate (ZnWO4) particles. The ZnWO4 particles were fabricated through a solid-state reaction between zinc oxide and tungsten oxide at various temperatures, producing particles with average sizes of 176.4 nm, 626.7 nm, and 2.127 μm; the zinc oxide and tungsten oxide were created using anodization. The spatial resolutions of high-resolution X-ray images, obtained from utilizing the fabricated particles, were determined: particles with the average size of 176.4 nm produced the highest spatial resolution. The results demonstrate that high spatial resolution can be obtained from ZnWO4 nanoparticle scintillators that minimize optical diffusion by having a particle size that is smaller than the emission wavelength.


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