Solid-state MAS NMR resonance assignment methods for proteins

2018 ◽  
Vol 106-107 ◽  
pp. 37-65 ◽  
Author(s):  
Victoria A. Higman
Keyword(s):  
Solid State ◽  
Resonance Assignment ◽  
Nmr Resonance Assignment ◽  
Mas Nmr

Assigning large proteins in the solid state: a MAS NMR resonance assignment strategy using selectively and extensively 13C-labelled proteins

2009 ◽  
Vol 44 (4) ◽  
pp. 245-260 ◽  
Author(s):  
Victoria A. Higman ◽  
Jeremy Flinders ◽  
Matthias Hiller ◽  
Stefan Jehle ◽  
Stefan Markovic ◽  
...  
Keyword(s):  
Solid State ◽  
Resonance Assignment ◽  
Nmr Resonance Assignment ◽  
Mas Nmr ◽  
Large Proteins ◽  
Assignment Strategy

scholarly journals Solid-state [13C–15N] NMR resonance assignment of hepatitis B virus core protein

2018 ◽  
Vol 12 (1) ◽  
pp. 205-214 ◽  
Author(s):  
Lauriane Lecoq ◽  
Shishan Wang ◽  
Thomas Wiegand ◽  
Stéphane Bressanelli ◽  
Michael Nassal ◽  
...  
Keyword(s):  
Hepatitis B Virus ◽  
Solid State ◽  
Hepatitis B ◽  
Resonance Assignment ◽  
Core Protein ◽  
Nmr Resonance Assignment ◽  
15N Nmr ◽  
Virus Core ◽  
B Virus

Fast Resonance Assignment and Fold Determination of Human Superoxide Dismutase by High-Resolution Proton-Detected Solid-State MAS NMR Spectroscopy

2011 ◽  
Vol 123 (49) ◽  
pp. 11901-11905 ◽  
Author(s):  
Michael J. Knight ◽  
Amy L. Webber ◽  
Andrew J. Pell ◽  
Paul Guerry ◽  
Emeline Barbet-Massin ◽  
...  
Keyword(s):  
Superoxide Dismutase ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Resonance Assignment ◽  
Mas Nmr

scholarly journals 13C Spin Dilution for Simplified and Complete Solid-State NMR Resonance Assignment of Insoluble Biological Assemblies

2011 ◽  
Vol 133 (13) ◽  
pp. 4722-4725 ◽  
Author(s):  
Antoine Loquet ◽  
Guohua Lv ◽  
Karin Giller ◽  
Stefan Becker ◽  
Adam Lange
Keyword(s):  
Solid State ◽  
Resonance Assignment ◽  
Solid State Nmr ◽  
Nmr Resonance Assignment

Fast Resonance Assignment and Fold Determination of Human Superoxide Dismutase by High-Resolution Proton-Detected Solid-State MAS NMR Spectroscopy

2011 ◽  
Vol 50 (49) ◽  
pp. 11697-11701 ◽  
Author(s):  
Michael J. Knight ◽  
Amy L. Webber ◽  
Andrew J. Pell ◽  
Paul Guerry ◽  
Emeline Barbet-Massin ◽  
...  
Keyword(s):  
Superoxide Dismutase ◽  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Resonance Assignment ◽  
Mas Nmr

Combining Multinuclear High-Resolution Solid-State MAS NMR and Computational Methods for Resonance Assignment of Glutathione Tripeptide

2012 ◽  
Vol 116 (25) ◽  
pp. 6711-6719 ◽  
Author(s):  
Mariana Sardo ◽  
Renée Siegel ◽  
Sérgio M. Santos ◽  
João Rocha ◽  
José R. B. Gomes ◽  
...  
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Computational Methods ◽  
Resonance Assignment ◽  
Mas Nmr

scholarly journals Automated solid-state NMR resonance assignment of protein microcrystals and amyloids

2013 ◽  
Vol 56 (3) ◽  
pp. 243-254 ◽  
Author(s):  
Elena Schmidt ◽  
Julia Gath ◽  
Birgit Habenstein ◽  
Francesco Ravotti ◽  
Kathrin Székely ◽  
...  
Keyword(s):  
Solid State ◽  
Resonance Assignment ◽  
Solid State Nmr ◽  
Nmr Resonance Assignment

The Nature of Chemisorbed CO2 in Zeolite A

2019 ◽  
Author(s):  
Przemyslaw Rzepka ◽  
Zoltán Bacsik ◽  
Andrew J. Pell ◽  
Niklas Hedin ◽  
Aleksander Jaworski
Keyword(s):  
Solid State ◽  
Ir Spectroscopy ◽  
Quantum Chemical Calculations ◽  
Quantum Chemical ◽  
Surface Coverage ◽  
Gas Mixtures ◽  
Mas Nmr ◽  
Significant Fraction ◽  
Zeolite A

Formation of CO<sub>3</sub><sup>2-</sup> and HCO<sub>3</sub><sup>-</sup> species without participation of the framework oxygen atoms upon chemisorption of CO<sub>2</sub> in zeolite |Na<sub>12</sub>|-A is revealed. The transfer of O and H atoms is very likely to have proceeded via the involvement of residual H<sub>2</sub>O or acid groups. A combined study by solid-state <sup>13</sup>C MAS NMR, quantum chemical calculations, and <i>in situ</i> IR spectroscopy showed that the chemisorption mainly occurred by the formation of HCO<sub>3</sub><sup>-</sup>. However, at a low surface coverage of physisorbed and acidic CO<sub>2</sub>, a significant fraction of the HCO<sub>3</sub><sup>-</sup> was deprotonated and transformed into CO<sub>3</sub><sup>2-</sup>. We expect that similar chemisorption of CO<sub>2</sub> would occur for low-silica zeolites and other basic silicates of interest for the capture of CO<sub>2</sub> from gas mixtures.

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