Fabrication and evaluation of an organic monolithic column based upon the polymerisation of hexyl methacrylate with 1,6-hexanediol ethoxylate diacrylate for the separation of small molecules by capillary liquid chromatography

Talanta ◽  
2015 ◽  
Vol 141 ◽  
pp. 103-110 ◽  
Author(s):  
Wael Alshitari ◽  
Cristina Legido Quigley ◽  
Norman Smith
Keyword(s):  
Liquid Chromatography ◽  
Small Molecules ◽  
Monolithic Column ◽  
Capillary Liquid Chromatography ◽  
Hexyl Methacrylate ◽  
Capillary Liquid

Preparation of a poly(3′-azido-3′-deoxythymidine-co-propargyl methacrylate-co-pentaerythritol triacrylate) monolithic column by in situ polymerization and a click reaction for capillary liquid chromatography of small molecules and proteins

The Analyst ◽  
2015 ◽  
Vol 140 (13) ◽  
pp. 4626-4635 ◽  
Author(s):  
Zian Lin ◽  
Ruifang Yu ◽  
Wenli Hu ◽  
Jiangnan Zheng ◽  
Ping Tong ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Free Radical ◽  
Small Molecules ◽  
In Situ Polymerization ◽  
Click Reaction ◽  
Monolithic Column ◽  
Capillary Liquid Chromatography ◽  
Pentaerythritol Triacrylate ◽  
Capillary Liquid

Combining free radical polymerization with a CuAAC click reaction, a facile approach was developed for the preparation of poly(AZT-co-PMA-co-PETA) monoliths.

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