Preparation of a poly(3′-azido-3′-deoxythymidine-co-propargyl methacrylate-co-pentaerythritol triacrylate) monolithic column by in situ polymerization and a click reaction for capillary liquid chromatography of small molecules and proteins

The Analyst ◽  
2015 ◽  
Vol 140 (13) ◽  
pp. 4626-4635 ◽  
Author(s):  
Zian Lin ◽  
Ruifang Yu ◽  
Wenli Hu ◽  
Jiangnan Zheng ◽  
Ping Tong ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Free Radical ◽  
Small Molecules ◽  
In Situ Polymerization ◽  
Click Reaction ◽  
Monolithic Column ◽  
Capillary Liquid Chromatography ◽  
Pentaerythritol Triacrylate ◽  
Capillary Liquid

Combining free radical polymerization with a CuAAC click reaction, a facile approach was developed for the preparation of poly(AZT-co-PMA-co-PETA) monoliths.

One-pot synthesis of polymer monolithic column by combination of free radical polymerization and azide–alkyne cycloaddition “click” reaction and its application in capillary liquid chromatography

RSC Advances ◽  
2015 ◽  
Vol 5 (13) ◽  
pp. 9828-9836 ◽  
Author(s):  
Ruifang Yu ◽  
Wenli Hu ◽  
Guo Lin ◽  
Qi Xiao ◽  
Jiangnan Zheng ◽  
...  
Keyword(s):  
Free Radical ◽  
Radical Polymerization ◽  
Click Reaction ◽  
Monolithic Column ◽  
Free Radical Polymerization ◽  
Capillary Liquid Chromatography ◽  
One Pot ◽  
Polymer Monoliths ◽  
Polymer Monolithic Column ◽  
Capillary Liquid

A facile “one-pot” method was developed for the preparation of polymer monoliths by combination of free radical polymerization and CuAAC click reaction.

Facile one-pot preparation of chiral monoliths with a well-defined framework based on the thiol–ene click reaction for capillary liquid chromatography

RSC Advances ◽  
2016 ◽  
Vol 6 (30) ◽  
pp. 24835-24842 ◽  
Author(s):  
Peng Zhang ◽  
Jiannan Wang ◽  
Haiguan Yang ◽  
Linjing Su ◽  
Yuhao Xiong ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Click Reaction ◽  
Capillary Liquid Chromatography ◽  
Fused Silica ◽  
One Pot ◽  
Fused Silica Capillary ◽  
Capillary Liquid ◽  
Silica Capillary

A novel chiral cyclodextrin (CD) monolith was easily prepared via a one-pot process based on the thiol–ene click reaction of allyl-β-CD with pentaerythritol tetra-(3-mercaptopropionate) in a fused-silica capillary.

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