The External Ion Microbeam of the LABEC Laboratory in Florence: Some Applications to Cultural Heritage

2011 ◽  
Vol 17 (5) ◽  
pp. 661-666 ◽  
Author(s):  
Silvia Calusi

AbstractIon beam analysis (IBA) techniques are a powerful analytical tool used to investigate the composition and structure of precious materials principally because they can be applied in atmosphere. Thus, the sample can be analyzed as is, and heating and charging effects are strongly diminished. Since IBA measurements can be made with low ion currents and acquisition time, the damage risk is limited. At the microbeam line of the LABEC laboratory, it is possible to exploit the potentials of IBA techniques in an external set up to reconstruct the distribution maps of all the detected elements over the analyzed area with spatial resolutions as low as 10 μm. This is an important feature when objects with inhomogeneous structures—on a scale of hundred microns or so—are investigated, as happens in some cases with artworks. The detection set up installed on our external microbeam allows us to use different IBA techniques simultaneously. Thus, in a single measurement run, it is possible to obtain complementary information on both sample composition and structure. Some applications to works of art are presented here as examples of the analytical capabilities of the external scanning microbeam in the cultural heritage field.

ACTA IMEKO ◽  
2017 ◽  
Vol 6 (3) ◽  
pp. 76 ◽  
Author(s):  
Alessandro Lo Giudice ◽  
Alessandro Re ◽  
Debora Angelici ◽  
Jacopo Corsi ◽  
Gianluca Gariani ◽  
...  

<p class="Abstract">Ion Beam Analyses (IBA) techniques, for example PIXE (Particle Induced X-ray Emission) and IL (IonoLuminescence), are a powerful analytical tool used to investigate the composition and structure of materials in cultural heritage. These techniques could be applied both in vacuum preparing the sample as in electron microscopy and in the air in a non-invasive way allowing to analyse artworks of practically any shape and dimension without sample preparation. Moreover the use of a focused beam (microbeam) permits to reach an analysis resolution of few micrometers in vacuum and ten micrometers in air.</p>In this work, instruments and methodologies are described and two examples of case study are reported: I) the mapping of elemental distribution in ancient roman coins; II) the trace elements measurement in lapis lazuli for provenance determination


1995 ◽  
Vol 05 (04) ◽  
pp. 249-253
Author(s):  
R.J. UTUI ◽  
N.P.O. HOMMAN ◽  
K.G. MALMQVIST

A new Ion Beam Analysis (IBA) facility which was recently installed in the Department of Physics of the Eduardo Mondlane University of Maputo, Mozambique, is described. The set up is based on a low energy (500 keV) Van de Graaff proton accelerator and is intended to be used in particle induced X-ray emission (PIXE), Rutherford Backscattering (RBS) and nuclear reaction analysis (NRA). Preliminary experiments on beam diagnostics were performed successfully and the followed procedure is described.


2008 ◽  
Vol 92 (1) ◽  
pp. 43-50 ◽  
Author(s):  
J. Salomon ◽  
J.-C. Dran ◽  
T. Guillou ◽  
B. Moignard ◽  
L. Pichon ◽  
...  

Author(s):  
T. Calligaro ◽  
J.-C. Dran ◽  
B. Moignard ◽  
L. Pichon ◽  
J. Salomon ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document