Capabilities of Single Particle Inductively Coupled Plasma Mass Spectrometry for the Size Measurement of Nanoparticles: A Case Study on Gold Nanoparticles

2014 ◽  
Vol 86 (7) ◽  
pp. 3405-3414 ◽  
Author(s):  
Jingyu Liu ◽  
Karen E. Murphy ◽  
Robert I. MacCuspie ◽  
Michael R. Winchester
Keyword(s):  
Mass Spectrometry ◽  
Gold Nanoparticles ◽  
Single Particle ◽  
Inductively Coupled Plasma ◽  
Size Measurement ◽  
Inductively Coupled ◽  
Plasma Mass Spectrometry

Graphene/gold nanoparticle composites for ultrasensitive and versatile biomarker assay using single-particle inductively-coupled plasma/mass spectrometry

The Analyst ◽  
2020 ◽  
Vol 145 (24) ◽  
pp. 7932-7940
Author(s):  
Yuqian Xing ◽  
Juan Han ◽  
Xu Wu ◽  
David T. Pierce ◽  
Julia Xiaojun Zhao
Keyword(s):  
Mass Spectrometry ◽  
Gold Nanoparticles ◽  
Gold Nanoparticle ◽  
Single Particle ◽  
Inductively Coupled Plasma ◽  
Inductively Coupled ◽  
Plasma Mass Spectrometry ◽  
Nanoparticle Composites

An ultrasensitive biomarker assay platform established by monitoring the gold nanoparticles (AuNPs) desorbed away from graphene triggered by the target using single-particle inductively-coupled plasma/mass spectrometry (spICP-MS).

scholarly journals Capabilities of fast data acquisition with microsecond time resolution in inductively coupled plasma mass spectrometry and identification of signal artifacts from millisecond dwell times during detection of single gold nanoparticles

2016 ◽  
Vol 31 (1) ◽  
pp. 135-144 ◽  
Author(s):  
I. Strenge ◽  
C. Engelhard
Keyword(s):  
Mass Spectrometry ◽  
Gold Nanoparticles ◽  
Data Acquisition ◽  
Time Resolution ◽  
Single Particle ◽  
Inductively Coupled Plasma ◽  
Inductively Coupled ◽  
Fast Data Acquisition ◽  
Icp Ms ◽  
Plasma Mass Spectrometry

In this paper, a home-built DAQ featuring microsecond time resolution is used to demonstrate advantages of fast data acquisition and to uncover potential artifacts in single-particle ICP-MS.

scholarly journals ANALYTICAL METHOD VALIDATION FOR THE IDENTIFICATION AND QUANTIFICATION OF DISSOLVED GOLD AND GOLD NANOPARTICLES IN COSMETICS PRODUCTS BY SINGLE PARTICLE INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY

Química Nova ◽  
2021 ◽  
Author(s):  
Lisia Santos ◽  
Cristiane Barata-Silva ◽  
Santos Vicentini Neto ◽  
Mayssa Fonseca ◽  
Carolina Magalhães ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Gold Nanoparticles ◽  
Single Particle ◽  
Inductively Coupled Plasma ◽  
Limit Of Detection ◽  
Concentration Limit ◽  
Inductively Coupled ◽  
Consumer Safety ◽  
Relative Standard ◽  
Plasma Mass Spectrometry

Nanoparticle (NP) applications have recently gained more space in the development of many products, especially in cosmetology. The aim of the present study was to validate a single particle inductively coupled plasma mass spectrometry technique for the detection and quantification of gold nanoparticles (AuNPs) and gold ions (Au (i)) in different cosmetics currently marketed in Brazil. The size limit of detection for pure AuNPs was 22 nm, and a concentration limit of detection of 2.3×106 particles g−1 was achieved. The limit of detection for total gold was 0.02 µg L−1 obtained in standard mode conditions. The recovery achieved was 98% for dissolved Au and 109% for AuNPs; the relative standard deviation was <5%. This validated method was applied to cosmetic products (n = 10) from different national and international industrial producers. Most cosmetics analysed contained quantifiable amounts of dissolved gold (< 0.005-2.1 µg g−1) and only four contained quantifiable amounts AuNPs the variability of the results detected (< LOD – 9.3 × 108 particles g−1). The products that contained the greatest amount of these metallic NPs were the artisanal products. The results demonstrate the importance of adequate quality control for cosmetics to ensure consumer safety

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