Hydrothermal Synthesis of (C6N2H14)2(UVI2UIVO4F12), a Mixed-Valent One-Dimensional Uranium Oxyfluoride

2000 ◽  
Vol 39 (17) ◽  
pp. 3791-3798 ◽  
Author(s):  
Simon Allen ◽  
Stephen Barlow ◽  
P. Shiv Halasyamani ◽  
J. Frederick W. Mosselmans ◽  
Dermot O'Hare ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
One Dimensional

ChemInform Abstract: Hydrothermal Synthesis and Structure of a New One-Dimensional, Mixed-Metal U(VI) Iodate, Cs2 [(UO2)(CrO4)(IO3)2].

ChemInform ◽  
2010 ◽  
Vol 33 (27) ◽  
pp. no-no
Author(s):  
Richard E. Sykora ◽  
Daniel M. Wells ◽  
Thomas E. Albrecht-Schmitt
Keyword(s):  
Hydrothermal Synthesis ◽  
One Dimensional ◽  
Mixed Metal

A New Type of Coordination Polymer: Hydrothermal Synthesis, Crystal Structure, and Magnetic Properties of [(C10H8N2)2CuBr]Cu3Br4

1998 ◽  
Vol 547 ◽  
Author(s):  
Brenda R. Cabrera ◽  
Ru-Ji Wang ◽  
Jing Li ◽  
Tan Yuen
Keyword(s):  
Hydrothermal Synthesis ◽  
Structure Type ◽  
X Ray Diffraction ◽  
Monoclinic System ◽  
One Dimensional ◽  
X Ray ◽  
Paramagnetic Behavior ◽  
Cell Dimensions ◽  
Susceptibility Study ◽  
New Type

AbstractGrowth of [(C10H8N2)2CuBr]Cu3Br4(I) crystals was achieved using the hydrothermal synthesis. Single crystal X-ray diffraction analysis shows that this compound crystallizes in monoclinic system, space group P21/c (no. 14) with four formula units in the unit cell. The cell dimensions are the following: a = 16.769(2) Å, b = 23.873(6) Å, c = 6.523(2) Å, β = 98.37(3)°, V = 2584(1) Å3. The title compound represents a new structure type. It consists of one-dimensional ribbons of 1[(Cu3Br4)] extending along the c-axis and discrete [(C10H8N2)2CuBr]+ complexes. The magnetic susceptibility study indicates a paramagnetic behavior due to the Cu(II) in the complex cations. The effective paramagnetic moment was calculated to be 2.20 μB from fitting the χ(T) data.

Hydrothermal synthesis and structure of one-dimensional Co(dien)2(VO3)3·(H2O) (dien=diethylenetriamine)

2003 ◽  
Vol 660 (1-3) ◽  
pp. 181-186 ◽  
Author(s):  
Bi-Zhou Lin ◽  
Zhen Li ◽  
Xiao-Ke Pei ◽  
Pei-De Liu
Keyword(s):  
Hydrothermal Synthesis ◽  
One Dimensional

Synthesis of One-Dimensional Chalcogenides by a Novel Hydrothermal Process

2004 ◽  
Vol 99-100 ◽  
pp. 203-208 ◽  
Author(s):  
Hui Zhang ◽  
De Ren Yang ◽  
Yujie Ji ◽  
Xiang Yang Ma ◽  
Jin Xu ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Critical Role ◽  
Hydrothermal Process ◽  
Nucleation And Growth ◽  
Saed Pattern ◽  
Orthorhombic Structure ◽  
X Ray Diffraction ◽  
One Dimensional ◽  
X Ray ◽  
Selected Area Electron Diffraction

A TGA assisted hydrothermal process was employed to prepare chalcogenide nanorods. The different morphology of CdS nanomaterials prepared with and without the TGA assisted hydrothermal process indicates that TGA plays a critical role in controlling the nucleation and growth of CdS nanomaterials. The paper makes a preliminary presentation of the mechanisms of preparation of chalcogenide nanostructures with and without the use of the TGA assisted hydrothermal synthesis. FeS nanorods and nanoparticles have been prepared by the TGA assisted and without the TGA assisted hydrothermal process, respectively, which confirmed the proposed mechanism. X-ray diffraction (XRD) shows that the nanorods are of orthorhombic structure, and selected area electron diffraction (SAED) pattern showed that the FeS nanorods were single crystalse. Further investigation for the synthesis of other chalcogenides will be undertaken in order to confirm the proposed mechanism.

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