Reactions of HC.tplbond.CCMe2NHCOR alkynes with M3(CO)12 carbonyl (M = Ru, R = C6H9, Ph; M = Os, R = C6H9). Synthesis and crystal structure of Ru4(CO)11(HC.tplbond.CCMe2NHCOC6H9), a butterfly cluster showing an interaction between a wingtip metal and the amide CO

1990 ◽  
Vol 9 (6) ◽  
pp. 1729-1734 ◽  
Author(s):  
Giovanni Predieri ◽  
Antonio Tiripicchio ◽  
Marisa Tiripicchio Camellini ◽  
Mirco Costa ◽  
Enrico Sappa
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure ◽  
Butterfly Cluster

Synthesis and Crystal Structure of a New Butterfly Cluster [Rh2Co2 (CO)6(μ-CO)4(μ4,η2-HC≡CFeCp2)]

2002 ◽  
Vol 2002 (7) ◽  
pp. 328-329
Author(s):  
Bao-Hua Zhu ◽  
Bin Hu ◽  
Wei-Qiang Zhang ◽  
Yuan-Qi Yin ◽  
Jie Sun
Keyword(s):  
Crystal Structure ◽  
Single Crystal ◽  
X Ray Diffraction ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Butterfly Cluster

The new butterfly cluster [Rh2Co2(CO)6(μ-CO)4(μ4, η2-HC≡CFeCp2)] 3 was obtained by the reaction of [Rh2Co2(CO)12] 1 with the 1-alkyne ligand HC≡CFeCp2 2, and the structure of cluster 3 has been established by single-crystal X-ray diffraction methods.

Synthesis and crystal structure of [MnL(μ-Cl)MnCl3]·H2O L=N, N'-bis(2'-pyridine)methyl-1,10-phenanthroline-2,9-dimethanamine

2002 ◽  
Vol 2002 (3) ◽  
pp. 120-121
Author(s):  
Tian Fu Liu ◽  
Hua Kuan Lin ◽  
Shou Rong Zhu ◽  
Zhong Ming Wang ◽  
Hong Gen Wang ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure

Synthesis and crystal structure of an 18-Mo girdle-like polyoxomolybdate

2002 ◽  
Vol 2002 (3) ◽  
pp. 107-109 ◽  
Author(s):  
Guang Liu ◽  
Jian Liu ◽  
Shi-Wei Zhang
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure

The Synthesis and Crystal Structure of Aluminum Selenite Trihydrate, Al2(seO3)3.32O

1992 ◽  
Author(s):  
W. T. Harrison ◽  
G. D. Stucky ◽  
R. E. Morris ◽  
A. K. Cheetham
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure

scholarly journals High-pressure synthesis and crystal structure of the mixed-cation borate Ga4In4B15O33(OH)3

2019 ◽  
Vol 74 (4) ◽  
pp. 357-363
Author(s):  
Daniela Vitzthum ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Mixed Cation ◽  
High Pressure High Temperature ◽  
Pressure Synthesis

AbstractThe mixed cation triel borate Ga4In4B15O33(OH)3 was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined via single-crystal X-ray diffraction data. Ga4In4B15O33(OH)3 crystallizes in the tetragonal space group I41/a (origin choice 2) with the lattice parameters a = 11.382(2), c = 15.244(2) Å, and V = 1974.9(4) Å3. The structure of the quaternary triel borate consists of a complex network of BO4 tetrahedra, edge-sharing InO6 octahedra in dinuclear units, and very dense edge-sharing GaO6 octahedra in tetranuclear units.

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