A nickel hydroxide platform prepared on hydroxyl-enriched screen-printed carbon electrode for oxidative electrocatalysis

2021 ◽  
Author(s):  
NEERAJAA SITHINI T ◽  
THIYAGASUNDARAM T ◽  
Jyh-Myng Zen

We report here the preparation of activation-free Ni electrode (i.e., eventually to the formation of NiOOH) through the enrichment of hydroxyl functional group via base-catalyzed hydrolysis reaction on “preanodized” screen...

2015 ◽  
pp. 84-90
Author(s):  
Nuzulul Kurniawan Isvani ◽  
Ani Mulyasuryani ◽  
Sasangka Prasetyawan

The performance of biosensor is based on the hydrolysis reaction of organophosphorus compounds catalyzed by organophosphate hydrolase (OPH), produce H+ and the other ionic species that increase conductance on the surface of electrode. In this research, OPH was immobilized by crosslinking on chitosan–glutaraldehyde membrane on the (Screen Printed Carbon Electrode) SPCE surface. Measurements were carried out at the range concentration 0 to 3.0 ppm of organophosphate, the range of pH 7.0 to 9.0 and 5–25 mL of enzyme. The result showed that optimum performances were obtained at 25 mL of OPH, pH 8.5, with the sensitivity for dizinon, malathion, chlorpirifos and profenofos is 1.353 mS/ppm, 1.270 mS/ppm, 1.230 mS/ppm dan 1.77 mS/ppm respectively and 0.97; 1.03; 0.98; 0.97 of LOD. DOI :http://dx.doi.org/10.15408/jkv.v0i0.3156.


2012 ◽  
Vol 571 ◽  
pp. 56-59
Author(s):  
Yu Fang Sha ◽  
Mei Zhao ◽  
Ming Quan Yang ◽  
Hai Xin Bai ◽  
Man Zhao

Biological multilayer films of redox polymer and horseradish peroxidase (HRP) were successfully assembled on a screen-printed carbon electrode using layer-by-layer (LBL) assembled method based on the electrostatic interaction. The screen-printed carbon electrode surface was modified by the positively charged redox polymer, and the negatively charged HRP by LBL method.


2021 ◽  
pp. 130574
Author(s):  
P.E. Resmi ◽  
Jeethu Raveendran ◽  
P.V. Suneesh ◽  
T. Ramanchandran ◽  
Bipin G Nair ◽  
...  

2014 ◽  
Vol 447 ◽  
pp. 162-168 ◽  
Author(s):  
Nicolaj Cruys-Bagger ◽  
Hirosuke Tatsumi ◽  
Kim Borch ◽  
Peter Westh

Talanta ◽  
2012 ◽  
Vol 88 ◽  
pp. 432-438 ◽  
Author(s):  
Julien Biscay ◽  
Estefanía Costa Rama ◽  
María Begoña González García ◽  
A. Julio Reviejo ◽  
José Manuel Pingarrón Carrazón ◽  
...  

Sensors ◽  
2018 ◽  
Vol 18 (12) ◽  
pp. 4324 ◽  
Author(s):  
Nurul Talib ◽  
Faridah Salam ◽  
Yusran Sulaiman

Clenbuterol (CLB) is an antibiotic and illegal growth promoter drug that has a long half-life and easily remains as residue and contaminates the animal-based food product that leads to various health problems. In this work, electrochemical immunosensor based on poly(3,4-ethylenedioxythiophene)/graphene oxide (PEDOT/GO) modified screen-printed carbon electrode (SPCE) for CLB detection was developed for antibiotic monitoring in a food product. The modification of SPCE with PEDOT/GO as a sensor platform was performed through electropolymerization, while the electrochemical assay was accomplished while using direct competitive format in which the free CLB and clenbuterol-horseradish peroxidase (CLB-HRP) in the solution will compete to form binding with the polyclonal anti-clenbuterol antibody (Ab) immobilized onto the modified electrode surface. A linear standard CLB calibration curve with R2 = 0.9619 and low limit of detection (0.196 ng mL−1) was reported. Analysis of milk samples indicated that this immunosensor was able to detect CLB in real samples and the results that were obtained were comparable with enzyme-linked immunosorbent assays (ELISA).


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