Laser heating setup for diamond anvil cells for in situ synchrotron and in house high and ultra-high pressure studies

2019 ◽  
Vol 90 (10) ◽  
pp. 104501 ◽  
Author(s):  
T. Fedotenko ◽  
L. Dubrovinsky ◽  
G. Aprilis ◽  
E. Koemets ◽  
A. Snigirev ◽  
...  
Keyword(s):  
High Pressure ◽  
Laser Heating ◽  
Diamond Anvil Cells ◽  
Ultra High Pressure ◽  
High Pressure Studies ◽  
Diamond Anvil

scholarly journals Synthesis of Manganese Mononitride with Tetragonal Structure under Pressure

Crystals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 511
Author(s):  
Dajian Huang ◽  
Caoping Niu ◽  
Bingmin Yan ◽  
Bo Gao ◽  
Lailei Wu ◽  
...  
Keyword(s):  
High Pressure ◽  
Phase Space ◽  
Laser Heating ◽  
Diamond Anvil Cell ◽  
Ambient Pressure ◽  
Tetragonal Structure ◽  
Metal Nitrides ◽  
Transition Metal Nitrides ◽  
Diamond Anvil

The exploration of the vast phase space of transition metal nitrides is critical for discovering novel materials and potential technological applications. Manganese mononitride with a tetragonal structure (space group I4/mmm) was synthesized in a laser-heating diamond anvil cell, which could be quenched to ambient pressure. The bulk modulus of 173 GPa was measured using in situ high-pressure diffraction, and the axial compressibility shows that, under pressure, the a direction is much more compressible than the c direction in tetragonal MnN. DFT results with correction of the on-site repulsion (GGA + U) confirm that tetragonal MnN is energetically stable and antiferromagnetic. This study highlights the need to include on-site repulsion to understand 3d metal nitrides.

scholarly journals Table-top nuclear magnetic resonance system for high-pressure studies with in situ laser heating

2019 ◽  
Vol 90 (12) ◽  
pp. 123901 ◽  
Author(s):  
Thomas Meier ◽  
Anand Prashant Dwivedi ◽  
Saiana Khandarkhaeva ◽  
Timofey Fedotenko ◽  
Natalia Dubrovinskaia ◽  
...  
Keyword(s):  
Nuclear Magnetic Resonance ◽  
High Pressure ◽  
Magnetic Resonance ◽  
Laser Heating ◽  
Resonance System ◽  
Magnetic Resonance System ◽  
High Pressure Studies ◽  
Nuclear Magnetic

Combined resistive and laser heating technique for in situ radial X-ray diffraction in the diamond anvil cell at high pressure and temperature

2013 ◽  
Vol 84 (2) ◽  
pp. 025118 ◽  
Author(s):  
Lowell Miyagi ◽  
Waruntorn Kanitpanyacharoen ◽  
Selva Vennila Raju ◽  
Pamela Kaercher ◽  
Jason Knight ◽  
...  
Keyword(s):  
High Pressure ◽  
Laser Heating ◽  
Diamond Anvil Cell ◽  
X Ray Diffraction ◽  
High Pressure And Temperature ◽  
X Ray ◽  
Diamond Anvil

scholarly journals Strategies forin situlaser heating in the diamond anvil cell at an X-ray diffraction beamline

2013 ◽  
Vol 21 (1) ◽  
pp. 89-96 ◽  
Author(s):  
Sylvain Petitgirard ◽  
Ashkan Salamat ◽  
Pierre Beck ◽  
Gunnar Weck ◽  
Pierre Bouvier
Keyword(s):  
High Pressure ◽  
Nd:Yag Laser ◽  
Laser Heating ◽  
Diamond Anvil Cell ◽  
X Ray Diffraction ◽  
Time Resolved ◽  
Pulsed Nd:Yag Laser ◽  
X Ray ◽  
Diamond Anvil

An overview of several innovations regardingin situlaser-heating techniques in the diamond anvil cell at the high-pressure beamline ID27 of the European Synchrotron Radiation Facility is presented. Pyrometry measurements have been adapted to allow simultaneous double-sided temperature measurements with the installation of two additional online laser systems: a CO2and a pulsed Nd:YAG laser system. This reiteration of laser-heating advancements at ID27 is designed to pave the way for a new generation of state-of-the-art experiments that demand the need for synchrotron diffraction techniques. Experimental examples are provided for each major development. The capabilities of the double pyrometer have been tested with the Nd:YAG continuous-wave lasers but also in a time-resolved configuration using the nanosecond-pulsed Nd:YAG laser on a Fe sample up to 180 GPa and 2900 K. The combination of time-resolved X-ray diffraction within situCO2laser heating is shown with the crystallization of a high-pressure phase of the naturally found pyrite mineral MnS2(11 GPa, 1100–1650 K).

High-pressure studies of the cubic to rhombohedral transformation in NbO2F

2000 ◽  
Vol 33 (4) ◽  
pp. 1175-1176 ◽  
Author(s):  
Stefan Carlson
Keyword(s):  
High Pressure ◽  
Bulk Modulus ◽  
Rhombohedral Phase ◽  
Cubic Phase ◽  
Diamond Anvil Cells ◽  
X Ray ◽  
High Pressure Studies ◽  
Diamond Anvil

ThePm\bar{3}mtoR\bar{3}chigh-pressure transition of NbO2F has been studied in detail using diamond anvil cells and synchrotron X-ray radiation. The transition starts at 0.28 GPa and is complete at 0.65 GPa. The bulk modulus for the cubic phase became 24.8 (11) GPa, which is roughly two times higher than for the rhombohedral phase.

In situ high pressure-temperature Raman spectroscopy technique with laser-heated diamond anvil cells

2004 ◽  
Vol 75 (10) ◽  
pp. 3302-3306 ◽  
Author(s):  
Jung-Fu Lin ◽  
Mario Santoro ◽  
Viktor V. Struzhkin ◽  
Ho-kwang Mao ◽  
Russell J. Hemley
Keyword(s):  
Raman Spectroscopy ◽  
High Pressure ◽  
Spectroscopy Technique ◽  
Diamond Anvil Cells ◽  
Diamond Anvil ◽  
Laser Heated
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