Rapid Determination of Warfarin by Sequential Injection Analysis with Cyclodextrin-Enhanced Fluorescence Detection

1998 ◽  
Vol 31 (5) ◽  
pp. 891-901 ◽  
Author(s):  
Lian X. Tang ◽  
Frederick J. Rowell
Talanta ◽  
2009 ◽  
Vol 79 (4) ◽  
pp. 1104-1110 ◽  
Author(s):  
Wanida Laiwattanapaisal ◽  
Usakorn Kunanuvat ◽  
Wichabhorn Intharachuti ◽  
Chakorn Chinvongamorn ◽  
Supot Hannongbua ◽  
...  

Talanta ◽  
2021 ◽  
Vol 231 ◽  
pp. 122355
Author(s):  
Timothy J. Trinklein ◽  
Malati Thapa ◽  
Lexie A. Lanphere ◽  
John A. Frost ◽  
Sandra M. Koresch ◽  
...  

2012 ◽  
Vol 03 (02) ◽  
pp. 131-137
Author(s):  
Yuwadee Boonyasit ◽  
Chakorn Chinvongamorn ◽  
Orawon Chailapakul ◽  
Wanida Laiwattanapaisal

1997 ◽  
Vol 80 (1) ◽  
pp. 25-30 ◽  
Author(s):  
Catharina Y W Ang ◽  
Luo Wenhong

Abstract A rapid and sensitive liquid chromatographic (LC) method was developed for the determination of am- picillin residues in raw bovine milk, processed skim milk, and pasteurized, homogenized whole milk with vitamin D. Milk samples were deprote- inized with trichloroacetic acid (TCA) and acetonitrile. After centrifugation, the clear supernatant was reacted with formaldehyde and TCA under heat. The major fluorescent derivative of ampicillin was then determined by reversed-phase LC with fluorescence detection. Average recoveries of ampicillin fortified at 5,10, and 20 ppb (ng/mL) were all >85% with coefficients of variation <10%. Limits of detection ranged from 0.31 to 0.51 ppb and limits of quantitation, from 0.66 to 1.2 ppb. After appropriate validation, this method should be suitable for rapid analysis of milk for ampicillin residues at the tolerance level of 10 ppb.


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