Preparation and Characterization of Nickel Oxide Nanostructures via Solid State Thermal Decomposition Approach

Author(s):  
Robabeh Mehdizadeh ◽  
Soheila Sanati ◽  
Lotf Ali Saghatforoush
2021 ◽  
Vol 127 (11) ◽  
Author(s):  
Eman Absi ◽  
Muneer Saleh ◽  
Naif Mohammed Al-Hada ◽  
Khaidzir Hamzah ◽  
Abdulsalam M. Alhawsawi ◽  
...  

2007 ◽  
Vol 72 (12) ◽  
pp. 1281-1293 ◽  
Author(s):  
Vukadin Leovac ◽  
Zoran Tomic ◽  
Katalin Mészáros-Szécsényi ◽  
Ljiljana Jovanovic ◽  
Milan Joksovic

The crystal and molecular structures of four tetrahedral structurally similar [Co(aamp)2X2] complexes (aamp = 4-acetyl-3-amino-5-methylpyrazole, X = Cl, Br, I and NCS) were determined by X-ray diffraction analysis and are discussed in detail. It was found that the different capacity of the ligand X (NCS vs. Cl, Br, I) for the formation of non-bonding contacts influence the mode of molecular association in the solid state. The complexes were characterized by UV-Vis spectroscopy. The first step of the thermal decomposition of the compounds was checked and is discussed in the view of the IR spectrum of the intermediate isolated from [Co(aamp)2Br2] by the quasi-isothermal technique.


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