CAPILLARY ELECTROPHORETIC BEHAVIOUR AND DETERMINATION OF ENOXACIN IN PHARMACEUTICAL PREPARATIONS AND HUMAN SERUM

2001 ◽  
Vol 24 (16) ◽  
pp. 2455-2467 ◽  
Author(s):  
Muzaffer Tunçel ◽  
Dilek Dogrukol-Ak ◽  
Zühre Sentürk ◽  
Sibel A. Özkan ◽  
Hassan Aboul-Enein
Keyword(s):  
Human Serum ◽  
Pharmaceutical Preparations ◽  
Capillary Electrophoretic

Spectrofluorimetric determination of tobramycin in human serum and pharmaceutical preparations by derivatization with fluorescamine

Luminescence ◽  
2013 ◽  
Vol 29 (1) ◽  
pp. 87-91 ◽  
Author(s):  
Serife Evrim Kepekci Tekkeli ◽  
Armağan Önal ◽  
A.Olcay Sağırlı
Keyword(s):  
Human Serum ◽  
Pharmaceutical Preparations ◽  
Spectrofluorimetric Determination

Determination of estradiol valerate in pharmaceutical preparations and human serum by flow injection chemiluminescence

Luminescence ◽  
2012 ◽  
Vol 28 (3) ◽  
pp. 407-411 ◽  
Author(s):  
Wenwen Liu ◽  
Liangxiao Xie ◽  
Hongshuang Liu ◽  
Shichao Xu ◽  
Bingcheng Hu ◽  
...  
Keyword(s):  
Human Serum ◽  
Flow Injection ◽  
Pharmaceutical Preparations ◽  
Estradiol Valerate ◽  
Flow Injection Chemiluminescence

scholarly journals A diperiodatoargentate(III)-based chemiluminescence determination of mitoxantrone in pharmaceutical preparations and human serum

2021 ◽  
Vol 14 (2) ◽  
pp. 393-401
Author(s):  
Lili Xue ◽  
Min Zhang ◽  
Guanghui Li ◽  
Jianhua Cao ◽  
Hanchun Yao
Keyword(s):  
Human Serum ◽  
Pharmaceutical Preparations

Capillary electrophoretic determination of sanguinarine and chelerythrine in plant extracts and pharmaceutical preparations

2000 ◽  
Vol 866 (2) ◽  
pp. 293-298 ◽  
Author(s):  
Juraj Ševčı́k ◽  
Jaroslav Vičar ◽  
Jitka Ulrichová ◽  
Ivo Válka ◽  
Karel Lemr ◽  
...  
Keyword(s):  
Plant Extracts ◽  
Pharmaceutical Preparations ◽  
Capillary Electrophoretic ◽  
Sanguinarine And Chelerythrine

scholarly journals Differential pulse voltammetric determination of diclofenac in pharmaceutical preparations and human serum

2015 ◽  
Vol 51 (2) ◽  
pp. 285-294 ◽  
Author(s):  
Bilal Yilmaz ◽  
Selcuk Kaban ◽  
Bilge Kagan Akcay ◽  
Ulvihan Ciltas
Keyword(s):  
Human Serum ◽  
Supporting Electrolyte ◽  
Pharmaceutical Preparation ◽  
Pharmaceutical Preparations ◽  
Differential Pulse ◽  
Acetonitrile Solution ◽  
Serum Samples ◽  
Electro Oxidation ◽  
Endogenous Substances

<p>This article describes a differential pulse voltammetric (DPV) method for the determination of diclofenac in pharmaceutical preparations and human serum. The proposed method was based on electro-oxidation of diclofenac at platinum electrode in 0.1 M TBAClO<sub>4</sub>/acetonitrile solution. The well-defined two oxidation peaks were observed at 0.87 and 1.27 V, respectively. Calibration curves that obtained by using current values measured for second peak were linear over the concentration range of 1.5-17.5 μg mL<sup>-1</sup>and 2-20 μg mL<sup>-1</sup> in supporting electrolyte and serum, respectively. Precision and accuracy were also checked in all media. Intra- and inter-day precision values for diclofenac were less than 3.87, and accuracy (relative error) was better than 4.12%. The method developed in this study is accurate, precise and can be easily applied to Diclomec, Dicloflam and Voltaren tablets as pharmaceutical preparation. In addition, the proposed technique was successfully applied to spiked human serum samples. No electro-active interferences from the endogenous substances were found in human serum.</p>

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