The Use of Flame Photometry For the Quantitative Determination of Sodium and Potassium in Plasma and Urine*

1949 ◽  
Vol 19 (5_ts) ◽  
pp. 461-470 ◽  
Author(s):  
Robert E. Mosher ◽  
A. J. Boyle ◽  
Edward J. Bird ◽  
S. D. Jacobson ◽  
Thomas M. Batchelor ◽  
...  
1956 ◽  
Vol 2 (2) ◽  
pp. 112-116 ◽  
Author(s):  
R L Dryer

Abstract A method for the determination of serum sodium and potassium involving only a single serum dilution is described. Samples of 0.1 ml. of serum suffice for both determinations, but larger samples may also be used. By careful control of the lithium concentration and the dilution factor the mean relative photometric error may be held to no more than 1 per cent under normal circumstances of operation.


1979 ◽  
Vol 10 (6) ◽  
pp. 613-614
Author(s):  
A. M. Volodina ◽  
V. I. Yakutin ◽  
A. K. Dibrova

1973 ◽  
Vol 56 (1) ◽  
pp. 184-187
Author(s):  
Brunetto Bazzi ◽  
Riccardo Fabbrini ◽  
Marco Radice

Abstract O,O-Dimethyldithiophosphoric acid and its alkaline salts are separated from impurities in technical preparations by thin layer chromatography on silica gel H, using 2 solvent systems: n-hexane-acetone and isopropanol-ammonium hydroxide. The plate is sprayed with palladium chloride for detection of the compounds. The area is scraped off and the compounds contained in this area are bromometrically titrated for quantitative determination. Good recoveries were obtained for O,O-dimethyldithiophosphoric acid and its sodium and potassium salts in pure samples and technical preparations.


2016 ◽  
Vol 12 (3-4) ◽  
Author(s):  
Vesna Gojković ◽  
Maja Šalić ◽  
Vesna Antunović ◽  
Goran Vučić ◽  
Željka Marjanović-Balaban

In the course of this study, we have determined the content of mineral matter of calcium, chlorides, sodium and potassium, by means of volumetric and instrumental analysis methods in infusion solutions. Infusion solutions that we used for analysis were purchased commercially in pharmacies in the Republic of Srpska. We have used volumetric methods, complexometry to determine calcium and Mohr method to determine chloride. Sodium and potassium were determined instrumentally, by flame photometry. Calcium was also determined by this method. The aim of the study was to demonstrate that the concentration of the aforementioned elements in infusion solutions corresponds to concentrations indicated on the label. Obtained results for content of sodium and chlorides do not deviate for more than allowed ±5%, in all three samples. Deviations occurred when content of calcium and potassium was determined by flame photometry.


1953 ◽  
Vol 30 (1) ◽  
pp. 1-17
Author(s):  
J. A. RAMSAY ◽  
R. H. J. BROWN ◽  
S. W. H. W. FALLOON

1. A method of flame photometry is described, by which the amount of sodium and potassium in biological fluids can be determined simultaneously, using samples of the order of 10-3 cu.mm. 2. When the method is tested with quantities near the lower limits of detection (of the order 4 x 10-8 mg. sodium, 6 x 10-8 mg. potassium) the reproducibility, measured as standard deviation, is ±7 x 10-9 mg. sodium and ± 17 x 10-9 mg. potassium. 3. When larger quantities (up to certain limits) are used, the standard deviation is approximately ± 3 % of the quantity in the sample, both for sodium and for potassium. 4. As is usual in flame photometry serious errors can be caused by the presence of other substances in the sample. In the case studied for purposes of illustration it is shown that these interference errors can be reduced to the order of ± 6 % by the addition of excess ammonium phosphate.


1981 ◽  
Vol 53 (4) ◽  
pp. 752-752
Author(s):  
S Farwell ◽  
D Liebowitz ◽  
R Kagel ◽  
D Adams
Keyword(s):  

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