scholarly journals Characterization of an in-vacuum PILATUS 1M detector

2014 ◽  
Vol 21 (3) ◽  
pp. 529-536 ◽  
Author(s):  
Jan Wernecke ◽  
Christian Gollwitzer ◽  
Peter Müller ◽  
Michael Krumrey
Keyword(s):  
Energy Range ◽  
Momentum Transfer ◽  
Photon Energy ◽  
Small Angle ◽  
Grazing Incidence ◽  
Light Elements ◽  
X Ray ◽  
X Ray Scattering ◽  
Pixel Pitch

A dedicated in-vacuum X-ray detector based on the hybrid pixel PILATUS 1M detector has been installed at the four-crystal monochromator beamline of the PTB at the electron storage ring BESSY II in Berlin, Germany. Owing to its windowless operation, the detector can be used in the entire photon energy range of the beamline from 10 keV down to 1.75 keV for small-angle X-ray scattering (SAXS) experiments and anomalous SAXS at absorption edges of light elements. The radiometric and geometric properties of the detector such as quantum efficiency, pixel pitch and module alignment have been determined with low uncertainties. The first grazing-incidence SAXS results demonstrate the superior resolution in momentum transfer achievable at low photon energies.

scholarly journals Characterization of Lipid-Templated Silica and Hybrid Thin Film Mesophases by Grazing Incidence Small-Angle X-ray Scattering

Langmuir ◽  
2009 ◽  
Vol 25 (16) ◽  
pp. 9500-9509 ◽  
Author(s):  
Darren R. Dunphy ◽  
Todd M. Alam ◽  
Michael P. Tate ◽  
Hugh W. Hillhouse ◽  
Bernd Smarsly ◽  
...  
Keyword(s):  
Thin Film ◽  
Small Angle ◽  
Grazing Incidence ◽  
Hybrid Thin Film ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Characterization of Mo/Si soft X-ray multilayer mirrors by grazing-incidence small-angle X-ray scattering

Vacuum ◽  
2009 ◽  
Vol 84 (1) ◽  
pp. 19-25 ◽  
Author(s):  
P. Siffalovic ◽  
E. Majkova ◽  
L. Chitu ◽  
M. Jergel ◽  
S. Luby ◽  
...  
Keyword(s):  
Small Angle ◽  
Grazing Incidence ◽  
Multilayer Mirrors ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Combining imaging ellipsometry and grazing incidence small angle X-ray scattering for in situ characterization of polymer nanostructures

2009 ◽  
Vol 396 (1) ◽  
pp. 139-149 ◽  
Author(s):  
Volker Körstgens ◽  
Johannes Wiedersich ◽  
Robert Meier ◽  
Jan Perlich ◽  
Stephan V. Roth ◽  
...  
Keyword(s):  
Small Angle ◽  
Grazing Incidence ◽  
In Situ Characterization ◽  
X Ray ◽  
Imaging Ellipsometry ◽  
X Ray Scattering ◽  
Polymer Nanostructures ◽  
Ray Scattering

Anomalous Small-Angle X-Ray Scattering Characterization of Model Pressure Vessel Alloy Microstructures

1998 ◽  
Vol 540 ◽  
Author(s):  
Dale E. Alexander ◽  
B. J. Kestel ◽  
P. R. Jemian ◽  
G. R. Odette ◽  
D. Klingensmith ◽  
...  
Keyword(s):  
Photon Energy ◽  
Small Angle ◽  
Pressure Vessel ◽  
Annealed Sample ◽  
Scattered Intensity ◽  
X Ray ◽  
X Ray Scattering ◽  
Guinier Analysis ◽  
Ray Scattering

AbstractAnomalous small-angle x-ray scattering (ASAXS) experiments were performed at energies near the Mn-K and Fe-K absorption edges on an Fe-0.9 Cu wt.%-1.0 Mn wt.% alloy subjected to either annealing at 450°C, 24 hrs or irradiation with 10 MeV electrons to 0.5 mdpa at 300°C. A Guinier analysis of the net scattered intensity revealed scatterers with radii of 16.5.16.8 Å and 16.4.17.3 Å for the irradiated and annealed foils, respectively. The variation in net scattered intensity with photon energy in the annealed sample was consistent with scattering contrast variations expected for Cu-rich, Cu-Mn precipitates. Minimal variation in net intensity (scattering contrast) with energy determined that Cu-Mn precipitates were not detected in the irradiated sample.

Characterization of Submicron-scale Periodic Grooves by Grazing Incidence Ultra-small-angle X-ray Scattering

2007 ◽  
Vol 46 (No. 32) ◽  
pp. L773-L775 ◽  
Author(s):  
Yoshiyasu Ito ◽  
Katsuhiko Inaba ◽  
Kazuhiko Omote ◽  
Yasuo Wada ◽  
Susumu Ikeda
Keyword(s):  
Small Angle ◽  
Grazing Incidence ◽  
X Ray ◽  
X Ray Scattering ◽  
Submicron Scale ◽  
Ray Scattering

Characterization of polymer thin films with small‐angle X‐ray scattering under grazing incidence (GISAXS)

2002 ◽  
Vol 15 (5) ◽  
pp. 35-42 ◽  
Author(s):  
Detlef‐M. Smilgies ◽  
Peter Busch ◽  
Christine M. Papadakis ◽  
Dorthe Posselt
Keyword(s):  
Thin Films ◽  
Small Angle ◽  
Polymer Thin Films ◽  
Grazing Incidence ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Small angle X-ray scattering study of porosity variation in a styrene-divinylbenzene copolymer

1981 ◽  
Vol 46 (7) ◽  
pp. 1675-1681 ◽  
Author(s):  
Josef Baldrian ◽  
Božena N. Kolarz ◽  
Henrik Galina
Keyword(s):  
Small Angle ◽  
Structural Parameters ◽  
Two Phase ◽  
X Ray ◽  
Porosity Variation ◽  
Swelling Agent ◽  
X Ray Scattering ◽  
Styrene Divinylbenzene ◽  
Ray Scattering

Porosity variations induced by swelling agent exchange were studied in a styrene-divinylbenzene copolymer. Standard methods were used in the characterization of copolymer porosity in the dry state and the results were compared with related structural parameters derived from small angle X-ray scattering (SAXS) measurements as developed for the characterization of two-phase systems. The SAXS method was also used for porosity determination in swollen samples. The differences in the porosity of dry samples were found to be an effect of the drying process, while in the swollen state the sample swells and deswells isotropically.

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