Crystal structure of [(E)-({2-[3-(2-{(1E)-[(carbamothioylamino)imino]methyl}phenoxy)propoxy]phenyl}methylidene)amino]thiourea with an unknown solvate
2015 ◽
Vol 71
(7)
◽
pp. o530-o531
◽
Keyword(s):
The title molecule, C19H22N6O2S2, has crystallographically imposedC2symmetry, with the central C atom lying on the rotation axis. The O—C—C—C torsion angle for the central chain is −59.22 (16)° and the dihedral angle between the planes of the benzene rings is 75.20 (7)°. In the crystal, N—H...O and N—H...S interactions link the molecules, forming a three-dimensional network encompassing channels running parallel to thecaxis, which account for about 20% of the unit-cell volume. The contribution to the scattering from the highly disordered solvent molecules in these channels was removed with the SQUEEZE routine [Spek (2015).Acta Cryst. C71, 9–18] inPLATON. The stated crystal data forMr, μetc.do not take these into account.
2015 ◽
Vol 71
(12)
◽
pp. m223-m224
◽
Keyword(s):
2015 ◽
Vol 71
(10)
◽
pp. 1262-1265
2014 ◽
Vol 70
(12)
◽
pp. o1250-o1251
◽
Keyword(s):
2015 ◽
Vol 71
(12)
◽
pp. o935-o936
◽
Keyword(s):
2014 ◽
Vol 70
(12)
◽
pp. o1270-o1271
◽
Keyword(s):
2018 ◽
Vol 74
(1)
◽
pp. 83-87
Keyword(s):
2014 ◽
Vol 70
(12)
◽
pp. o1287-o1287
Keyword(s):
2020 ◽
Vol 76
(6)
◽
pp. 803-806
Keyword(s):
2014 ◽
Vol 70
(10)
◽
pp. 262-264
◽
Keyword(s):
2015 ◽
Vol 71
(12)
◽
pp. 1467-1470
Keyword(s):