Determination of Various Crystallite Parameter for ZNO Nanoparticles Under Compression

Author(s):  
Abu Yousuf ◽  
Rasel Mohammad Khokan ◽  
Tetsuo Soga ◽  
Amr Attia Abuelwafa ◽  
Md. Shamimul Hoque Choudhury ◽  
...  
Keyword(s):  
2016 ◽  
Vol 28 (5) ◽  
pp. 055704
Author(s):  
Clara Guglieri ◽  
Giuliana Aquilanti ◽  
Sofía Díaz-Moreno ◽  
J Chaboy

2021 ◽  
Vol 4 (01) ◽  
pp. 16-25
Author(s):  
Hamideh Asadollahzadeh

Zinc oxide (ZnO) nanoparticles with an average size of 60 nm have been successfully prepared by microwave irradiation. Carbon paste electrode (CPE) was modified with ZnO nanoparticles and used for the electrochemical oxidation of chlorpheniramine maleate (CPM). Cyclic voltammetry (CV) study of the modified electrode indicated that the oxidation potential shifted towards a lower potential by approximately 106 mV and the peak current was enhanced by 2 fold in comparison to the bare CPE (ZnO/CPE-CV). The electrochemical behaviour was further described by characterization studies of scan rate, pH and concentration of CPM. Under the optimal conditions, the peak current was proportional to CPM concentration in the range of 8.0 ×10-7 to 1.0 × 10-3 mol L-1 with a detection limit of 5.0 × 10-7 mol L-1 by differential pulse voltammetry (DPV). The peak current of CPM is linear in the concentration range of 0.8 - 1000 µM (R2=0.998). The ZnO/CPE has good reproducibility and high stability for the determination of CPM using this electrode. The proposed method was successfully applied to the determination of CPM in pharmaceutical samples. In addition, the important analytical parameters were compared with other methods which show that ZnO/CPE-CV procedure is comparable to recently reported methods.


2020 ◽  
Vol 12 (2) ◽  
Author(s):  
Tirza C. Raganata ◽  
Henry Aritonang ◽  
Edi Suryanto

ABSTRAKTelah dilakukan penelitian tentang fotokatalis metilen biru menggunakan nanopartikel ZnO yang disentisis dengan metode kopresipitasi. Kemampuan fotokatalis dilakukan terhadap zat warna methylene blue 5 ppm menggunakan fotokatalis ZnO yang disinari sinar UV-A selama 30, 60, 120, 150, dan 180 menit. Penentuan konsentrasi dihitung berdasarkan absorbansi yang didapatkan dari hasil Spektrofotometri UV-Vis dan dalam rumus menghitung % degradasi. Hasil penelitian menunjukkan bahwa yang memiliki kemampuan fotokatalis paling baik adalah Nanopartikel ZnO 10% yaitu dengan nilai persen degradasi untuk variasi waktu penyinaran 30 menit adalah sebesar 51,82%, 60 menit sebesar 65,26%, 120 menit sebesar 71,25%, 150 menit sebesar 75,78%, dan 180 menit sebesar 71,01%. Dan waktu penyinaran optimum terjadi pada waktu kontak 150 menit. ABSTRACTA research on photocatalysts of methylene blue using ZnO nanoparticles were analyzed using coprecipitation method. The ability of photocatalysts was carried out on 5 ppm methylene blue dyes using ZnO photocatalysts which were exposed to UV-A rays for 30, 60, 120, 150, and 180 minutes. Determination of concentration was calculated based on the absorbance obtained from the results of the UV-Vis Spectrophotometry test reading and in the formula to calculate% degradation. The results showed that the best photocatalysts ability was ZnO 10% nanoparticles, ie the percent degradation value for 30 minutes irradiation time variation was 51.82%, 60 minutes was 65.26%, 120 minutes was 71.25%, 150 minutes at 75.78%, and 180 minutes at 71.01%. And the optimum exposure time occurs at 150 minutes contact time. 


RSC Advances ◽  
2021 ◽  
Vol 11 (60) ◽  
pp. 37877-37885
Author(s):  
Sherin Rison ◽  
Rijo Rajeev ◽  
Vinay S. Bhat ◽  
Agnus T. Mathews ◽  
Anitha Varghese ◽  
...  

Electrochemically deposited ZnO nanoparticles on a pencil graphite electrode (PGE) coated with graphene generate a noteworthy conductive and selective electrochemical sensing electrode for the estimation of cortisol.


Author(s):  
Md. Shamimul Haque Choudhury ◽  
Md. Abdullah Al Masud ◽  
Md. Abirul Haque Chowdhury ◽  
Abu Yousuf ◽  
Mohammad Rafiqul islam ◽  
...  

2015 ◽  
Vol 19 (1/2) ◽  
Author(s):  
B. P. Rudyk ◽  
B. D. Nechyporuk ◽  
N. Yu. Novoseletskyy ◽  
V. A. Syaskyy ◽  
B. A. Tataryn

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