Experimental chemical shift correlation maps from heteronuclear two-dimensional nuclear magnetic resonance spectroscopy. II: Carbon-13 and proton chemical shifts of a-D-glucopyranose oligomers
1982 ◽
Vol 60
(19)
◽
pp. 2431-2441
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Keyword(s):
2D Nmr
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Double Fourier transform ("2D") nmr methods allow the simultaneous measurement of proton and carbon-13 chemical shifts for each directly bonded carbon–proton pair in a molecule. As well as greatly increasing the number of different resonances that may be distinguished in the spectra of complex systems, the measurement of correlated proton and carbon-13 shifts allows the otherwise inaccessible proton shifts to be determined, and facilitates the assignment of conventional proton and carbon-13 spectra. Results are presented for glucose, maltose, maltotriose, α-cyclodextrin, β-cyclodextrin, and dextran T-10; reassignments are proposed for the carbon-13 spectra of maltose and maltotriose.
1981 ◽
Vol 103
(16)
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pp. 4703-4711
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1981 ◽
Vol 42
(1)
◽
pp. 164-168
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2007 ◽
Vol 185
(2)
◽
pp. 240-246
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Keyword(s):
1966 ◽
Vol 70
(3)
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pp. 939-941
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1989 ◽
Vol 37
(6)
◽
pp. 612-615
1985 ◽
Vol 62
(3)
◽
pp. 543-550
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