The Catalyst for Growing Single-Walled Carbon Nanotubes by Catalytic Chemical Vapor Deposition Method

2009 ◽  
Vol 9 (4) ◽  
pp. 2480-2495 ◽  
Author(s):  
Avetik R. Harutyunyan
2004 ◽  
Vol 858 ◽  
Author(s):  
H. Emrah Unalan ◽  
Manish Chhowalla

ABSTRACTSingle-walled carbon nanotubes (SWNTs) were synthesized both in powder form and on substrates using alcohol catalytic chemical vapor deposition method (ACCVD). A detailed parametric study was conducted. As-grown SWNTs were analyzed using transmission electron microscopy (HRTEM), field-emission scanning electron microscopy (FE-SEM) and Raman spectroscopy. Nucleation and growth of SWNTs occurred within seconds after introduction of the alcohol vapor. The results show that high quality SWNTs with a narrow diameter distribution without amorphous carbon can be grown using Co acetate catalyst doped with Fe acetate above 750°C. Defective nanotubes were observed at low (450°C) and high (950°C) temperatures with the optimum temperature being 850°C. In brief, our work has taken a step towards optimizing SWNTs growth conditions using ACCVD.


2019 ◽  
Vol 55 (92) ◽  
pp. 13888-13891 ◽  
Author(s):  
Sook Young Moon ◽  
Woo Sik Kim

Highly oriented metallic and semiconducting SWCNTs were synthesized with different carrier gas compositions and etchant amounts by the floating catalyst chemical vapor deposition method.


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