04/02221 Catalytic synthesis of single-walled carbon nanotubes from coal gas by chemical vapor deposition method

2004 ◽  
Vol 45 (5) ◽  
pp. 317
2019 ◽  
Vol 55 (92) ◽  
pp. 13888-13891 ◽  
Author(s):  
Sook Young Moon ◽  
Woo Sik Kim

Highly oriented metallic and semiconducting SWCNTs were synthesized with different carrier gas compositions and etchant amounts by the floating catalyst chemical vapor deposition method.


2013 ◽  
Vol 662 ◽  
pp. 3-6
Author(s):  
Chang Yu ◽  
Xiang Tong Meng ◽  
Lei Zhang ◽  
Jie Shan Qiu

Double-walled carbon nanotubes (DWCNTs) have been synthesized by a floating catalytic chemical vapor deposition method (FC-CVD) in diameter-varied reactor with xylene as carbon sources, ferrocene as catalyst precursor, and sulfur as additive. The as-grown products were characterized by scanning electron microscope (SEM), transmission electron microscope (TEM), and Raman spectrometer. The results show that DWCNTs with a high graphite degree is centimeter-scale in length, and the inner diameter varies in the range of 1.5-1.7 nm. The effect of reactor diameter on the structure and morphology of the products was also investigated and compared. It is believed that the diameter-varied reactor may become a feasible route to the mass and continuous production of DWCNTs.


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