Investigation of Copper Etching with a Ferric Nitrate Solution

2019 ◽  
Vol 19 (10) ◽  
pp. 6347-6351
Author(s):  
Jeong-Soo Kim ◽  
Dongchul Suh
1987 ◽  
Vol 111 ◽  
Author(s):  
J. A. Sawicki ◽  
J. H. Rolston ◽  
S. R. Julian ◽  
T. Tyliszczak ◽  
K. D. McCrimmon

AbstractSpecimens of highly dispersed Pt/Silicalite catalyst, decorated with 57Fe by impregnation in aqueous ferric nitrate solution, have been studied after decoration, and various pretreatments including exposure to carbon monoxide, by in situ Mössbauer spectroscopy. The form of Pt was followed by EXAFS analysis near the Pt LIII edge. The microstructural studies were combined with CO chemisorption and infrared absorption measurements. It is observed that iron in Pt clusters is very reactive even at ambient temperatures and that the interaction of Fe with CO is strongly accelerated by platinum.


Nano Research ◽  
2018 ◽  
Vol 11 (8) ◽  
pp. 3959-3971 ◽  
Author(s):  
Huajie Yin ◽  
Lixue Jiang ◽  
Porun Liu ◽  
Mohammad Al-Mamun ◽  
Yun Wang ◽  
...  

2013 ◽  
Vol 772 ◽  
pp. 884-887 ◽  
Author(s):  
Xu Hui Sun ◽  
Lei Wang ◽  
Wen Chao Li ◽  
Wan Quan Tuo

Ferrate is a powerful oxidant and disinfectant that has been proposed for use in drinking water treatment for more than a decade. The main obstacles in the application are costs and stability. In water treatment, using wet oxidation method to prepare liquid ferrate can save production costs. Saturated ferric nitrate solution can get higher efficiency and productivity to generate ferrate. Water quality has no obvious effect on the productivity of ferrate. The optimum alkaline concentration is 10-13 mol/L. The reaction time and temperature affect the quality of liquid ferrate product. The larger the mole ratio of sodium hypochlorite to ferric nitrate is, the greater the productivity of ferrate is. The proportion of sodium hypochlorite to ferric nitrate should be adjusted appropriately.


2020 ◽  
Vol 81 (7) ◽  
pp. 1494-1506
Author(s):  
Maad F. Al Juboury ◽  
Musa H. Alshammari ◽  
Mohammed R. Al-Juhaishi ◽  
Laith A. Naji ◽  
Ayad A. H. Faisal ◽  
...  

Abstract To apply the principles of sustainability, this study aims to prepare the composite sorbent from mixing of solid wastes that resulted from activities of treatment plants for wastewater and water supply. The manufacturing process depends on the mixing of sewage sludge with waterworks sludge at different proportions and the best mixture is modified by ferric nitrate solution. The prepared composite sorbent was evaluated as permeable reactive barrier (PRB) in the capturing of methylene blue (MB) dye presented in the simulated groundwater. Results proved that the suitable mixture of composite sorbent consisting of 0.25 g sewage sludge with 0.75 g waterworks sludge coated with aqueous solution of 2 g of Fe(NO3)2 achieved the maximum sorption capacity. In comparison with Freundlich model, Langmuir expression described the sorption measurements in a well manner; so, the chemisorption is governed by the removal of MB with maximum adsorption capacity reached to 268.98 mg/g. Kinetic measurements could be more representative by pseudo-first-order model and this means that the sorption process is supported by physical forces. Finally, the effects of inlet concentrations and bed thickness on the migration of MB front were simulated in an efficient manner by COMSOL Multiphysics 3.5a package with root mean squared errors not in excess of 0.152.


1975 ◽  
Vol 21 (8) ◽  
pp. 1167-1168 ◽  
Author(s):  
Nagy A Farid ◽  
Gordon S Born ◽  
Wayne V Kessler ◽  
S M Shaw ◽  
W E Lange

Abstract We describe an improvement in the Levy and Procknal method [J. Pharm. Sci. 57, 1330 (1968)] for determination of salicylic acid and its metabolites in urine. Salicylic acid and salicyluric acid are successively extracted from 1 or 2 ml of urine (acidified with HCl) by two 10-ml portions each of carbon tetrachloride and ethylene dichloride. The extracts of each solvent are shaken with 5 ml of ferric nitrate solution (a 10-fold dilution of 17 g of Fe(NO3)3·9H2O in 1 liter of 70 mmol/liter HNO3). The aqueous phases are centrifuged and their absorbances measured at 530 nm. For total salicylate, 3 ml of urine and 3 ml of HCl are heated in a partially evacuated serum vial at 100 °C for 16 h and then salicylic acid is assayed in the hydrolyzed sample. Recovery of a weighed oral dose of sodium salicylate in urine was 105.4%; it was 127.9% by the Levy and Procknal method for the same sample. The improved method is faster and more accurate.


2013 ◽  
Vol 634-638 ◽  
pp. 2193-2197
Author(s):  
Hu Zhou ◽  
Jian Dong Zhuang ◽  
Qian Liu

Novel Fe3O4/ordered mesoporous carbon (OMC) composite powders have been prepared by impregnation and reduction methods for the microwave absorbing application purpose. The Fe3O4nanoparticles were encapsulated in the mesopores of OMCs, and Fe3O4contents in the composite could be easily controlled by changing the concentration of ferric nitrate solution during the preparation. The Fe3O4/OMC composites show very excellent microwave absorbing properties with respect to pure OMC samples, in a frequency ranging of 8.2-12.4 GHz. A minimum reflection loss (RL) value of -32 dB at 11.35 GHz and a broader absorption band with the RL values under -10 dB are obtained when the thickness of samples is 1.6 mm. The enhanced microwave absorption of the Fe3O4/OMC nanocomposites is contributed to the better impedance match between dielectric loss and magnetic loss, which originates from the incorporation of magnetic species into OMC.


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