Mode-I and mode-II interlaminar fracture properties of high modulus pitch-based carbon fiber reinforced polymers containing different nanostructures

2021 ◽  
pp. 002199832110492
Author(s):  
Kimiyoshi Naito ◽  
Chiemi Nagai

The mode-I and mode-II interlaminar fracture properties of high modulus pitch-based carbon fiber reinforced polymers (CFRPs) (fiber: K13C; resin: EX-1515 cyanate ester) modified with 20–30 nm β-SiC nanoparticles or multiwalled-carbon nanotubes (MWCNTs) were investigated. Different volume fractions of both the β-SiC nanoparticles (1, 2, 5, and 10 vol%) and MWCNTs (1, 3, 5, and 7 vol%) were tested. The values of the mode-I and mode-II interlaminar fracture toughness of the CFRPs containing the lowest volume fractions of these nanostructures were larger compared with the unfilled composite but decreased with increasing the volume fraction of the inclusions. No differences in mechanical properties were observed among the different nanostructure types.

2017 ◽  
Vol 742 ◽  
pp. 652-659
Author(s):  
Matthias Merzkirch ◽  
Louise Ahure Powell ◽  
Tim Foecke

Numerical models based on cohesive zones are usually used to model and simulate the mechanical behavior of laminated carbon fiber reinforced polymers (CFRP) in automotive and aerospace applications and require different interlaminar properties. The current work focuses on determining the interlaminar fracture toughness (GIC) under Mode I loading of a double cantilever beam (DCB) specimen of unidirectional CFRP, serving as prototypical material. The novelty of this investigation is the improvement of the testing methodology by introducing digital image correlation (DIC) as an extensometer and this tool allows for crack growth measurement, phenomenological visualization and quantification of various material responses to Mode I loading. Multiple methodologies from different international standards and other common techniques are compared for the determination of the evolution of GIC as crack resistance curves (R-curves). The primarily metrological sources of uncertainty, in contrast to material specific related uncertainties, are discussed through a simple sensitivity analysis. Additionally, the current work offers a detailed insight into the constraints and assumptions to allow exploration of different methods for the determination of material properties using the DIC measured data. The main aim is an improvement of the measurement technique and an increase in the reliability of measured data during static testing, in advance of future rate dependent testing for crashworthiness simulations.


2017 ◽  
Vol 52 (7) ◽  
pp. 945-952 ◽  
Author(s):  
Xin Liu ◽  
Tao Sun ◽  
Zhanjun Wu ◽  
Huiyong He

The nanosheet boehmite (AlOOH) was synthesized and used as reinforcing agent to toughen carbon fiber-reinforced polymers. The purity, morphology, size and composition of the AlOOH nanosheets were investigated by the methods of XRD, SEM, TEM and FTIR, respectively. Interlaminar fracture toughness for mode II deformation was investigated for carbon fiber-reinforced polymers toughened by AlOOH nanosheets varying the contents at room temperature (RT, 293k) and at low temperature (LT, 77k). The fracture surfaces were examined by SEM to correlate with the interlaminar fracture properties. The results indicated that the synthesized AlOOH nanosheets were pure crystalline and of high purity. By TEM, the thickness of the lamellar AlOOH sample is about 22 nm. The end-notched flexure test results show that interlaminar fracture toughness of unidirectional carbon fiber-reinforced polymer with the same content AlOOH nanosheets (0, 1, 1.5, 2, 2.5, 3 wt.%) at LT is higher than that at RT. The interlaminar fracture toughness reaches the highest when the AlOOH nanosheets content equals 2% at RT. But at LT, the highest interlaminar fracture toughness appeared in the carbon fiber-reinforced polymers without AlOOH nanosheets.


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