Optical Methods in Solid Mechanics

2017 ◽  
pp. 583-603
Author(s):  
Anand Asundi
1985 ◽  
Vol 38 (10) ◽  
pp. 1279-1281
Author(s):  
R. J. Clifton ◽  
F. P. Chiang

Mechanical failure of machine parts, structures, and microelectronic components has a strong negative impact on the safety, security, and productivity of our people. Prevention of these failures is a principal focus of solid mechanics, which uses analysis, experiment, and computation to provide the understanding necessary for failure reduction through improved design, fabrication, and inspection. Experimental mechanics plays a critical role in this effort since it provides the data base for the calculations and the means for testing the validity of proposed theoretical models of failure. Current trends in experimental mechanics show increased use of optical methods for monitoring the displacements, velocities, and strains of surfaces. This trend has gained impetus from the attractiveness of noncontact methods for hostile environments and dynamically loaded bodies. Advances in laser technology have enhanced the instrumentation associated with these methods. Another trend is the investigation of material behavior under more complex loading conditions, made possible by the availability of servo-controlled testing machines with computer interfaces. Still another trend is the increased attention given to defects, such as inclusions, cracks, and holes, because of their importance in failure mechanisms. Opportunities for future contributions from experimental mechanics appear to be great and to occur across a broad range of technological problems. A central theme of future research appears to be increased emphasis on measurements at the micron and submicron scale in order to advance the understanding of material response and failure at the micromechanical level. Increased attention will also be given to internal measurements of defects, deformations and residual stresses because of their importance in developing a fundamental understanding of failure. Automated data reduction and control of experiments will greatly increase the information obtained from experiments and its usefulness for the development of mathematical models. Other important research directions include improved methods for measurements of in situ stresses in rocks, improved measurements of displacements and physiological parameters in biological systems, capability for long-term monitoring of the integrity of structures, and improved sensors for feedback control of mechanical systems.


Author(s):  
A. Legrouri

The industrial importance of metal catalysts supported on reducible oxides has stimulated considerable interest during the last few years. This presentation reports on the study of the physicochemical properties of metallic rhodium supported on vanadium pentoxide (Rh/V2O5). Electron optical methods, in conjunction with other techniques, were used to characterise the catalyst before its use in the hydrogenolysis of butane; a reaction for which Rh metal is known to be among the most active catalysts.V2O5 powder was prepared by thermal decomposition of high purity ammonium metavanadate in air at 400 °C for 2 hours. Previous studies of the microstructure of this compound, by HREM, SEM and gas adsorption, showed it to be non— porous with a very low surface area of 6m2/g3. The metal loading of the catalyst used was lwt%Rh on V2Q5. It was prepared by wet impregnating the support with an aqueous solution of RhCI3.3H2O.


Author(s):  
H. Seiler ◽  
U. Haas ◽  
K.H. Körtje

The physical properties of small metal particles reveal an intermediate position between atomic and bulk material. Especially Ag has shown pronounced size effects. We compared silver layers evaporated in high vacuum with cluster layers of small silver particles, evaporated in N2 at a pressure of about 102 Pa. The investigations were performed by electron optical methods (TEM, SEM, EELS) and by Photoacoustic (PA) Spectroscopy (gas-microphone detection).The observation of cluster layers with TEM and high resolution SEM show small silver particles with diameters of about 50 nm (Fig. 1 and Figure 2, respectively). The electron diffraction patterns of homogeneous Ag layers and of cluster layers are similar, whereas the low loss EELS spectra due to plasmon excitation are quite different. Fig. 3 and Figure 4 show first results of EELS spectra of a cluster layer of small silver particles on carbon foil and of a homogeneous Ag layer, respectively.


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