Preparation and Characterisation of Iodo-functionalised Azobenzene Derivatives of the Type I–p-C6H4–N=N–p-C6H4–X
2008 ◽
Vol 63
(12)
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pp. 1395-1401
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A broad range of azobenzene derivates of the general type I-p-C6H4-N=N-p-C6H4-X (1) have been prepared. In the case of X = Ph (b), C≡C-Fc (e, Fc = ferrocenyl), OMe (g), Oi-Pr (i), and NMe2 (m), these compounds have been characterised by single-crystal X-ray structure analysis. In addition, the closely related 4-dimethylamino-1-(4-iodophenylazo)naphthalene 2 and 8-(4-iodophenylazo) quinoline 3 have also been prepared. Furthermore, the ferrocene derivative Fc-C≡C-p-C6H4- NH2 (4), which served as a starting material for the synthesis of I-p-C6H4-N=N-p-C6H4-p-C6H4- C≡C-Fc (1e), was prepared and structurally characterised by X-ray diffraction.
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2013 ◽
Vol 69
(4)
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pp. 334-336
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2012 ◽
Vol 36
(3)
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pp. 178-180
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1997 ◽
Vol 52
(5)
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pp. 573-576
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