Test Method for Major and Minor Elements in Coal and Coke Ash By X-Ray Fluorescence

Author(s):  
Keyword(s):  
X Ray ◽  
2014 ◽  
Vol 584-586 ◽  
pp. 894-898
Author(s):  
Ping Zhang ◽  
Guan Guo Liu ◽  
Chao Ming Pang ◽  
Bing Du ◽  
Hong Gen Qin

The X ray computed tomography (X-CT) was applied to test the cracking resistance of cement paste, and the hydration process was monitored to study the effect of fly ash on the early age cracking performance. The results showed that the hydration heat reduced with the increase of fly ash under the same water-cement ratio. Within 24h, the porosity increased with time. The addition of fly ash increased the proportion of large holes and then changed the internal stress state. Using X-CT test method and by comparing the number of cracks, the sample with 20% FA was found to have the most serious cracks, whereas the sample with 30% FA had the best crack resistance.


Author(s):  
Rajni Bhardwaj ◽  
Smita Johar ◽  
Amit Kapila ◽  
Amandeep Sharma

Swarnamakshika is grouped under Updhatu of Swarna and is composed of Copper, Iron and Sulphur. In this study Swarnamakshika was subjected to Shodhana by Bharjana with Nimbuka swarasa and Shudha Swarnamakshika was given Bhavana with Nimbuka swarasa and subjected to Varahaputa. With ten Varahaputa Bhasma Siddhi Lakshanas were attained swarnamakshika Marana was done by using Nimbuka swarasa until bhasma siddi lakshanas found and it took 10 puta till it attained reddish brown color. The X-ray diffraction analysis showed that d-identified peaks after 10th puta Swarnamakshika bhasma composition is of Iron oxide with rhombohedral crystal system as main component. EDX analysis of Swarna makshika bhasma shows that it contains Iron and Oxygen, as major element and Copper, Sulphur, Carbon, Aluminium, Calcium etc. as minor elements. FESEM study revealed that the particle size of Ashudha and Shudha Swarnamakshika was in the range of 500 nm-3nm. Keywords: Swarnamakshika Bhasma, Nimbuka swarasa, puta


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