Effect of temperature on the hydration of cement paste: composition, microstructure and properties

Author(s):  
J. F. Young
2007 ◽  
Vol 33 (8) ◽  
pp. 1503-1507 ◽  
Author(s):  
Guo-jun Li ◽  
Zhan-ru Sun ◽  
Hong Zhao ◽  
Chun-huan Chen ◽  
Rui-ming Ren

2005 ◽  
Vol 35 (3) ◽  
pp. 609-613 ◽  
Author(s):  
Lucia Alarcon-Ruiz ◽  
Gerard Platret ◽  
Etienne Massieu ◽  
Alain Ehrlacher

Materials ◽  
2019 ◽  
Vol 12 (13) ◽  
pp. 2098 ◽  
Author(s):  
Jan Weichhold ◽  
Uwe Gbureck ◽  
Friedlinde Goetz-Neunhoeffer ◽  
Katrin Hurle

A calcium deficient hydroxyapatite (CDHA) forming cement with a bimodal grain size distribution, composed of α-TCP and fine grained CDHA at a weight ratio of 9:1, was modified by the addition of sodium phytate (IP6) in variable amounts ranging from 0.25 to 2 wt.%, related to the powder content. The injectability of the cement paste was drastically increased by the IP6 addition, independent of the amount of added IP6. Additionally, the cement paste viscosity during the first minutes decreased. These effects could be clearly related to a slightly more negative zeta potential. Furthermore, IP6 was shown to strongly retard the setting reaction, as can be seen both in the calorimetry and X-ray diffraction measurements. In addition, octacalcium phosphate (OCP) was identified as a further setting product. All measurements were performed at 23 °C and 37 °C to assess the effect of temperature on the setting reaction for both clinical handling by the surgeon and the final hardening in the bone defect.


1986 ◽  
Vol 85 ◽  
Author(s):  
I. Odler ◽  
S. Abdul-Maula ◽  
Lu Zhongya

ABSTRACTThe effect of temperature on the progress of hydration and cement paste structure and properties was studied using four laboratory-synthesized portland cements, hydrated at temperatures between 5 and 95°C for up to 90 days. In addition to an accelerated progress of hydration, elevated temperatures altered the phase composition and pore structure of the resulting hydrated material. Below 75°C the effect of temperature on the intrinsic bond properties of the hydrates formed remained negligible.


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