The crystallization and optimization of magnetic properties effects in FeXSiB (X=Cu, V,
Co, Zr, Nb) amorphous alloys were studied by applying X-ray diffraction methods, high resolution
transmission electron microscopy (HRTEM), resistometric and magnetic measurements. The
temperatures of the first and the second stage of crystallization, the 1h optimization annealing
temperature and the Curie temperature were determined for different amorphous alloys. Activation
energies of crystallization process were obtained by applying the Kissinger method. The influence
of alloy additions on optimization effect and crystallization processes was carefully examined.