Differential Pulse Voltammetric Determination of Piroxicam on Lanthanide Ferric Oxide Nanoparticles-Carbon Paste Modified Electrode

2018 ◽  
Vol 14 (3) ◽  
pp. 271-276 ◽  
Author(s):  
Isaac Yves Lopes de Macedo ◽  
Morgana Fernandes Alecrim ◽  
Luane Ferreira Garcia ◽  
Aparecido Ribeiro de Souza ◽  
Wallans Torres Pio dos Santos ◽  
...  
2019 ◽  
Vol 84 (2) ◽  
pp. 175-185 ◽  
Author(s):  
Mohadeseh Safaei ◽  
Hadi Beitollahi ◽  
Masoud Shishehbore ◽  
Somayeh Tajik ◽  
Rahman Hosseinzadeh

A carbon paste electrode (CPE) was modified with N-(ferrocenylmethylidene) fluorene-2-amine and graphene/ZnO nanocomposite. The electrooxidation of captopril (CAP) at the surface of the modified electrode was studied using electrochemical approaches. The electrochemical study of the modified electrode, as well as its efficiency for the electrocatalytic oxidation of captopril, is described. The electrode was used to study the electrocatalytic oxidation of captopril, by cyclic voltammetry (CV), chronoamperometry (CHA) and differential pulse voltammetry (DPV) as diagnostic techniques. It has been found that the oxidation of captopril at the surface of modified electrode occurs at a potential of about 340 mV less positive than that of an unmodified CPE. DPV of captopril at the electrochemical sensor exhibited two linear dynamic ranges (0.1?100.0 and 100.0?800.0 ?M) with a detection limit (3?) of 0.05 ?M.


2010 ◽  
Vol 75 (5) ◽  
pp. 681-687 ◽  
Author(s):  
Zsigmond Papp ◽  
Valéria Guzsvány ◽  
Szymon Kubiak ◽  
Andrzej Bobrowski ◽  
Luka Bjelica

The objective of the work was to investigate the possibility of using a tricresyl phosphate-based carbon paste electrode for the direct voltammetric determination of the neonicotinoid insecticide thiamethoxam. The analyte was determined by differential pulse voltammetry in Britton-Robinson buffer pH 7.0 in the concentration range of 3.72 - 41.5 ?g mL-1. The reproducibility of the analytical signal at the 7.29 ?g mL-1 level was characterized by a relative standard deviation of 1.3 %. The applicability of the developed method was evaluated by determining thiamethoxam in a river water sample and a commercial formulation Actara 25 WG.


1999 ◽  
Vol 32 (5) ◽  
pp. 865-883 ◽  
Author(s):  
Gang Chen ◽  
Shuping Bi ◽  
Lemei Dai ◽  
Mi Cao ◽  
Yijun Chen ◽  
...  

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