Cycloaddition Reactions Assisted by Microwave Irradiation: Protic Ionic liquids vs Solvent-free Conditions

2017 ◽  
Vol 4 (3) ◽  
Author(s):  
Pedro M. E. Mancini ◽  
María N. Kneeteman ◽  
Mauro Cainelli ◽  
Carla M. Ormachea
Keyword(s):  
Ionic Liquids ◽  
Microwave Irradiation ◽  
Solvent Free ◽  
Cycloaddition Reactions ◽  
Protic Ionic Liquids ◽  
Solvent Free Conditions

scholarly journals Tandem Fries Reaction–Conjugate Addition under Microwave Irradiation in Dry Media; One-pot Synthesis of Flavanones

1999 ◽  
Vol 23 (9) ◽  
pp. 574-575
Author(s):  
Firouz Matloubi Moghaddam ◽  
Mohammad Ghaffarzadeh ◽  
Seyed Hossein Abdi-Oskoui
Keyword(s):  
Microwave Irradiation ◽  
Silica Gel ◽  
Conjugate Addition ◽  
Solvent Free ◽  
Naphthalene Derivatives ◽  
One Pot ◽  
Fries Rearrangement ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Fries Reaction

An AICl3–ZnCl2 mixture supported on silica gel is found to be an efficient medium for the Fries rearrangement of acyloxybenzene or naphthalene derivatives in solvent-free conditions under microwave irradiation.

scholarly journals TMSOTf-catalyzed synthesis of trisubstituted imidazoles using hexamethyldisilazane as a nitrogen source under neat and microwave irradiation conditions

RSC Advances ◽  
2021 ◽  
Vol 11 (45) ◽  
pp. 28061-28071
Author(s):  
Kesatebrhan Haile Asressu ◽  
Chieh-Kai Chan ◽  
Cheng-Chung Wang
Keyword(s):  
Microwave Irradiation ◽  
Nitrogen Source ◽  
Microwave Heating ◽  
Solvent Free ◽  
Solvent Free Conditions

Trisubstituted imidazoles are synthesized efficiently from the readily available 1,2-diketones and aldehydes using hexamethyldisilazane as a new and stable nitrogen source under TMSOTf-catalysis system, microwave heating and solvent-free conditions.

Microwave-assisted synthesis of quinolones and 4H-1,4-benzo thiazine 1,1-dioxides

2005 ◽  
Vol 2005 (1) ◽  
pp. 27-28 ◽  
Author(s):  
Jaime Charris ◽  
Arthur Barazarte ◽  
José Domínguez ◽  
Neira Gamboa
Keyword(s):  
Microwave Irradiation ◽  
Rapid Method ◽  
Solvent Free ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted ◽  
Solvent Free Conditions

A rapid method for the preparation of N-aryl-2-methylthio-4-oxo-1,4-dihydro quinoline-3-carbonitriles (2a–e) and N-aryl-3-methylthio-4H-1,4-benzothiazine-2-carbonitrile 1,1-dioxides (2f–o) is reported. The cyclization is accelerated by microwave irradiation under solvent free conditions in the presence of K2CO3.

Sign in / Sign up

Export Citation Format

Share Document