scholarly journals Synthesis of Metal Doped TiO2 Nano-Composites by Sol-Gel Method and Their Structural Properties

2020 ◽  
Vol 6 (3) ◽  
pp. 915-917
Author(s):  
Rajani Altaf ◽  
Sharma Jyoti ◽  
Dave Pranav
Keyword(s):  
Metal Oxide ◽  
Sol Gel ◽  
Nano Composites ◽  
Gel Method ◽  
Doped Tio2 ◽  
Sol Gel Method ◽  
Ir Studies ◽  
Good Crystallinity ◽  
Ft Ir ◽  
Metal Doped

Metal oxide nano-composites plays a very important role in many areas of chemistry, physics and material science. This paper explains the synthesis and comparison of zinc and zirconium doped TiO2 metal oxide nano-composites and their different properties. Here the sol-gel method is used to synthesis both the nano-composites. Nano-composites have been characterized with XRD, AFM, Zetasizer & potential and FT-IR studies. XRD study revealed good crystallinity with the size range of 30 nm – 45 nm for both nano-composites. AFM studies also revealed the same. FTIR study reports the characteristics peaks of synthesised nano-composites.

Preparation and Characterization of MgO Nanoparticles by Sol–Gel Method

2018 ◽  
Vol 24 (8) ◽  
pp. 5708-5711
Author(s):  
Nikhar Khanna ◽  
A. Ruban Kumar
Keyword(s):  
Surface Passivation ◽  
Sol Gel ◽  
Phase Method ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Ir Studies ◽  
Liquid Phase Method ◽  
Ft Ir ◽  
Size And Morphology

Liquid phase method (sol–gel method) was employed to synthesize MgO nanparticles. The particles were subjected to structural, morphological and optical property studies. X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform Infrared Spectroscopy (FT-IR), UV-Vis Spectrophotometer were employed to characterize the given sample. The X-ray pattern obtained had no impurity peak, revealing high purity of the sample. The particle size and morphology were investigated by SEM. EDS and FT-IR studies were done for knowing the composition and surface passivation respectively of the prepared sample. The estimation of the band-gap was carried out by UV-vis absorption spectra.

Study on photocatalytic degradation of gaseous dichloromethane using pure and iron ion-doped TiO2 prepared by the sol–gel method

Chemosphere ◽  
2007 ◽  
Vol 66 (11) ◽  
pp. 2142-2151 ◽  
Author(s):  
Wen-Chi Hung ◽  
Ssu-Han Fu ◽  
Jeou-Jen Tseng ◽  
Hsin Chu ◽  
Tzu-Hsing Ko
Keyword(s):  
Photocatalytic Degradation ◽  
Sol Gel ◽  
Iron Ion ◽  
Gel Method ◽  
Doped Tio2 ◽  
Sol Gel Method

scholarly journals Synthesis and Characterization of Boron, Copper, and Zinc-Doped Hydroxyapatite by Sol-Gel Method: Research of Absorption and Thermal Behavior

2021 ◽  
Author(s):  
Dilek Çanakçı
Keyword(s):  
Thermal Behavior ◽  
Sol Gel ◽  
Absorption Bands ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Copper And Zinc ◽  
Vis Spectroscopy ◽  
Metal Doped

Abstract In this study, hydroxyapatites reinforced with Boron, Copper and Zinc at different rates were produced using the sol-gel method. Different amounts of metal during the production of hydroxyapatite were used to observe the amount of crystallization and morphological differences in their structures. The characterization of the metal-doped HAp was carried out by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDX). The data indicated that the Ca/P stoichiometric ratios of the samples varied between 1.71 and 2, so their morphologies were different from each other. The absorption behavior of novel metal-doped HAp samples was evaluated at room temperature by UV-vis spectroscopy. In the absorption spectra of the samples, absorption bands formed in similar regions. In addition, the thermal behavior of HAp samples was investigated using TG/DTA techniques. The results of the analysis showed that heat resistance of the new synthesized samples was quite high.

Preparation of La0.75Sr0.25Cr0.5Mn0.5O3-δ Nanometer Powders by Sol-Gel Method and Research about its Electrochemical Performance

2013 ◽  
Vol 712-715 ◽  
pp. 257-261
Author(s):  
Yin Lin Wu ◽  
Qing Hui Wang ◽  
Ling Wang ◽  
Hai Yan Zhao
Keyword(s):  
Heat Treatment ◽  
Particle Size ◽  
Electrochemical Performance ◽  
Heat Treatment Temperature ◽  
Sol Gel ◽  
Treatment Temperature ◽  
Preparation Process ◽  
Gel Method ◽  
Sol Gel Method ◽  
Ft Ir

The La0.75Sr0.25Cr0.5Mn0.5O3-δnanometer powders were prepared by citric acid sol-gel method.The samples were characterized by DTA, FT-IR, XRD, TEM techniques. The preparation process, morphology of synthesized powders, the best heat-treatment temperature and the electrochemical performance had been studied. The results show that the spherical nanometer powders can be obtained and the best heat-treatment temperature is 800°C. The particle size is about 30nm and Ea is 0.071 eV.

scholarly journals Structural, optical, and magnetic study of Ni-doped TiO2 nanoparticles synthesized by sol–gel method

2018 ◽  
Vol 8 (1) ◽  
pp. 1-8 ◽  
Author(s):  
M. Manzoor ◽  
A. Rafiq ◽  
M. Ikram ◽  
M. Nafees ◽  
S. Ali
Keyword(s):  
Tio2 Nanoparticles ◽  
Sol Gel ◽  
Magnetic Study ◽  
Gel Method ◽  
Doped Tio2 ◽  
Sol Gel Method
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