scholarly journals Methods for obtaining a dispersed structure and increasing the strength of silicon-manganese steels

Author(s):  
Vladimir Bolshakov ◽  
Aleksandr Kalinin ◽  
Diana Hlushkova ◽  
Georgij Tohtar ◽  
Valeriy Bagrov ◽  
...  

For high-strength structural steels, the problem of grinding grain and increasing strength is solved by the use of highly efficient technologies, the development of new steel compositions and the development of rational thermomechanical processing. Goal. The aim of the work is to transform the structure, study the methods of grain grinding and increase the strength properties of structural steels 09Г2, 09Г2С as a result of modification by nanodisperse compositions, heat treatment and intense plastic deformation. Methodology. The research material was structural low-carbon steels 09G2, 09G2S. The process of modifying the steel parameters of the geometric shape of the melts was carried out by smelting steels 09G2 and 09G2C in an induction furnace. The modified workpieces were subjected to intensive plastic deformation and heat-treating treatment according to the mode: heating temperature 1050 °C, exposure 5 min; cooled medium: water and 20 % solution of NaCl in water. Then  – a rest at temperatures of 500 °C; 600 °C, exposure time – 30 minutes. Metallographic studies of the structure of steels before and after modification and mechanical testing of standard samples were performed. Results. The study of the structure grains of steels 09Г2 and 09Г2С in the initial state showed the presence of large grains up to 30 μm, reduced microhardness and yield strength. Originality. The substantiation of the choice of type and fraction of nanodisperse modifier was carried out. The use of plasma-chemical synthesis to obtain nanopowders based on titanium was substantiated. Nanopowders of titanium carbonitride Ti (CN) fraction 50 ... 100 nm were obtained by the method of plasma chemical synthesis. Practical value. The following methods were proposed for grinding grain and increasing the strength properties of steels: nanomodification, intensive plastic deformation in combination with heat-strengthening treatment.

2020 ◽  
Vol 864 ◽  
pp. 278-284
Author(s):  
Vladimir Bolshakov ◽  
Nataliia Kalinina ◽  
Diana Нlushkova ◽  
Igor Kіrichenko ◽  
Alexander Voronkov ◽  
...  

Crystallographic characteristics of nanodispersed materials obtained by plasma-chemical synthesis were studied. Using industrial equipment for plasma-chemical synthesis the nanodispersed powders of high-melting carbide, nitride, carbonitride and silicide class compounds based on titanium, magnesium, aluminium, silicon were obtained. Technology for synthesis of powder fraction less than 100 nm was developed. The efficiency of nanodisperce compositions use in smelting of structural steels was determined. In the result of 10Г2С steel modification with Ti (CN) nanopowder strength, plastic properties and impact toughness were improved. Elemental composition of nanodispersed composition was determined: SiC, TiC, TiN, Ti (CN), AlN, Mg2Si, Mg3N2. The elemental composition of synthesized compounds corresponded to stoichiometric composition. Microdiffractional patterns of the particles were analysed, it was shown that nanopowders belong to the solid crystalline bodies with metallic bond. It has been found, that titanium carbonitride Ti (CN) particles have face-centered and silicon carbide (SiC) particles have hexagonal crystal lattice. Experiments for steel 10Г2 and 10Г2С modifying with nanopowder compositions on base of Ti (CN) and SiC were carried out. The efficiency of nanodisperce compositions use in smelting of structural steels was determined. In the result of 10Г2С steel modification with Ti (CN) nanopowder strength, plastic properties and impact toughness were improved. The choice of nanodisperce titanium carbonitride Ti (CN) powders with 100 nm fraction for light alloy steels modifying was justified. The required criteria for choice of nanopowder modifiers were obtained: insolubility in smelt, correspondence of crystal lattice to steel matrix, commensurability with austenite germ critical radius in crystallizing.


2019 ◽  
Vol 2019 ◽  
pp. 1-6
Author(s):  
Galina Kholodnaya ◽  
Roman Sazonov ◽  
Denis Ponomarev ◽  
Igor Zhirkov

This paper presents a study on pulsed plasma-chemical synthesis of fluorine- and gold-doped silicon oxide nanopowder. The gold- and fluorine-containing precursors were gold chloride (AuCl3) and sulphur hexafluoride (SF6). Pulsed plasma-chemical synthesis is realized on the laboratory stand, including a plasma-chemical reactor and TEA-500 electron accelerator. The parameters of the electron beam are as follows: 400–450 keV electron energy, 60 ns half-amplitude pulse duration, up to 200 J pulse energy, and 5 cm beam diameter. We confirmed the composite structure of SixOy@Au by using transmission electron microscopy and energy-dispersive spectroscopy. We determined the chemical composition and morphology of synthesized SixOy@Au and SixOy@F nanocomposites. The material contained a SixOy@Au carrier with an average size of 50–150 nm and a shell of fine particles with an average size of 5–10 nm.


2021 ◽  
Vol 1870 (1) ◽  
pp. 012003
Author(s):  
B A Timerkaev ◽  
V S Felsinger ◽  
A A Kaleeva ◽  
E A Erlingayte ◽  
J A Uktamov ◽  
...  

2020 ◽  
Vol 15 (10) ◽  
pp. 709-712
Author(s):  
Galina Kholodnaya ◽  
Roman Sazonov ◽  
Denis Ponomarev ◽  
Alexander Sivkov ◽  
Ivan Shanenkov ◽  
...  

2012 ◽  
Vol 14 (11) ◽  
pp. 980-995 ◽  
Author(s):  
Katerina Zaharieva ◽  
Gheorghi Vissokov ◽  
Janis Grabis ◽  
Slavcho Rakovsky

2021 ◽  
Vol 12 (3) ◽  
pp. 638-642
Author(s):  
V. F. Shamray ◽  
A.V. Samokhin ◽  
V. P. Sirotinkin ◽  
A. G. Astashov ◽  
A. S. Gordeev

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