scholarly journals Instrumental Neutron Activation Analysis (INAA) of Cisadane Estuarine Sediments

2018 ◽  
Vol 10 (1) ◽  
pp. 58
Author(s):  
Ali Arman Lubis

Nuclear analytical technique instrumental neutron activation analysis was employed for the multielemental analysis of sediments collected from Cisadane estuary. This analytical technique provides concentration of 20 elementswhich consist of heavy metals and rare earth elements simultaneously. Two sediments cores were collected using core sampler for determining the distribution of all elements in the depth profiles of sediments. Sediment cores were subdivided into 2 cm increment, dried and sent to reactor for irradiation using thermal flux of ?1013 neutrons.cm-2.s-1 for 20 minutes in Research Reactor Siwabessy, National Nuclear Energy Agency (BATAN), Serpong. Irradiated samples were measured using a multichannel analyzer (MCA) gamma spectrometer coupled with high purity germanium detector. Analysis of particle size was done since uptake of heavy metals by sediments is particle-size dependent. The results are presented and discussed.

1997 ◽  
Vol 80 (4) ◽  
pp. 871-882 ◽  
Author(s):  
William C Cunningham ◽  
Stephen G Capar ◽  
David L Anderson

Abstract A formalized method for determining sodium in biological materials by instrumental neutron activation analysis is presented. The method includes common procedures from the numerous options available to this historically nonformalized analytical technique. The number of procedural options is restricted to minimize the method’s complexity, yet the method is still applicable to a variety of neutron activation facilities. High accuracy and precision are achieved by placing bounds on allowed uncertainty at critical stages of the analysis. Analytical results from the U.S. Food and Drug Administration laboratory and 4 other laboratories demonstrate the method’s performance.


1999 ◽  
Vol 77 (10) ◽  
pp. 1626-1637
Author(s):  
Robert Schutte ◽  
Gordon R Thompson ◽  
Kingsley K Donkor ◽  
M John M Duke ◽  
Roger Cowles ◽  
...  

Instrumental neutron activation analysis (INAA) was used to predict the relative amounts of various sizes of fine particles in Athabasca oil sands. The method is based on regression analysis of element concentration data for 529 oil sand test portions, determined by INAA, against particle size distributions determined by three currently used methods. The most important elements for the estimation of particle sizes below 44 µm were found to be aluminum, sodium, and manganese. The INAA estimation method works because variation in elemental composition within particle size fractions in oil sands up to at least 44 µm is relatively small, whereas the variation between size fractions is significant. The new method does not involve the use of organic solvents, is faster and simpler to perform than the methods currently in use, and is comparable in precision. It has the added advantages that it can be readily automated, and concentrations of elements of special interest in oil sand processing, such as chlorine, are obtained simultaneously.Key words: instrumental neutron activation analysis, oil sand, particle size distribution.


2016 ◽  
Vol 5 (03) ◽  
pp. 4892 ◽  
Author(s):  
Ratna Raju M.* ◽  
Madhusudhana Rao P. V. ◽  
Seshi Reddy T. ◽  
Raju M. K. ◽  
Brahmaji Rao J. S. ◽  
...  

A study was undertaken to evaluate the inorganic elements for humans in two Indian medicinal plants leaves, namely Sphaeranthus indicus, and Cassia fistula by Instrumental Neutron Activation Analysis (INAA). INAA experiment was performed by using 20 kW KAMINI Reactor at Indira Gandhi Centre for Atomic Research (IGCAR), Kalpakkam. The emitted gamma rays were measured using gamma ray spectrometer. The concentrations of Al, Br, Ca, Fe, K, La, Mg, Mn, Na, Sc, V and Zn were determined in the selected medicinal plants. The medicinal leaves are using in treatment of various important ailments. The elemental content in selected medicinal leaves is various proportions depending on the soil composition, location of plant specimen and the climate in which the plant grows.


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