Oilseed residues. Determination of total residual hexane

1995 ◽  

1972 ◽  
Vol 55 (6) ◽  
pp. 1226-1227
Author(s):  
Mark A Litchman ◽  
Lewis A Turano ◽  
Ronald P Upton

Abstract A method is described for the quantitative determination of hexane in modified hop extract by head-space gas-liquid chromatography. A sample of extract is weighed into a serum vial and water-methanol solution is added. The vial is sealed tightly and heated 1 hr in a 70°C bath. A sample of the head-space gas over the solution is injected onto a Porapak Q gas chromatographic column for determination. Recovery of 2–29 ppm hexane added to potassium isohumulone was 95.5–114.8%. The method may be applicable to other hop extracts.



1954 ◽  
Vol 2 (4) ◽  
pp. 202-203 ◽  
Author(s):  
D. A. Mapes ◽  
S. A. Shrader




1972 ◽  
Vol 49 (2) ◽  
pp. 129-131 ◽  
Author(s):  
Sara P. Fore ◽  
H. P. Dupuy




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