A Surface-Enhanced Resonance Raman Scattering Method for the Determination of Trace Crystal Violet on Colloidal Au Nanoparticle Substrate

2013 ◽  
Vol 299 ◽  
pp. 191-194 ◽  
Author(s):  
Zhi Liang Jiang ◽  
Lu Ma ◽  
Ai Hui Liang

Colloidal Au nanoparticles as active substrate for surface-enhanced resonance Raman scattering(SERRS) were prepared by the trisodium citrate-reduced procedure. In pH 6.6 Na2HPO4-NaH2PO4 buffer solution and in the presence of aggregation reagent NaCl, nanogolds were aggregated to form stable aggregated- nanogolds (ANG). The crystal violet (CV) adsorbed on the surface of ANG to form CV-ANG conjugates that produce strongest surface-enhanced resonance Raman scattering peak at 1616 cm-1. In the optimal condition, the SERRS intensity at 1616 cm-1 was linear to the CV concentration in the range of 2.5×10-8 -1.75×10-7 mol/L, a surface-enhanced resonance Raman scattering assay was set up for detection of trace CV, with good selectivity.

2013 ◽  
Vol 647 ◽  
pp. 181-184
Author(s):  
Yan Yan Wei ◽  
Fang Li ◽  
Ai Hui Liang ◽  
Zhi Liang Jiang

A stable nanosilver solution was prepared, using PEG10000 as stabilizer and NaBH4 as reducer. In pH 6.6 Na2HPO4-NaH2PO4 buffer solution containing PEG10000 and NaCl, nanosilvers were aggregated to form the stable aggregated-nanosilvers (ANS) that could conjugate with 4-mercaptopyridine (MP) to produce an ANS-MP surface-enhanced resonance Raman scattering (SERRS) probe, which exhibited a strong SERS peak at 1097 cm-1. When cystine (Cy) concentration increased, the SERS intensity at 1097 cm-1 decreased linearly. In the optimal condition, the decreased SERRS intensity was linear to Cy concentration in the range of 5.0×10-9-1.4×10-7 mol/L, with a detection limit of 2.0×10-9 mol/L Cy.


2013 ◽  
Vol 664 ◽  
pp. 32-36
Author(s):  
Yan Yan Wei ◽  
Gui Qing Wen ◽  
Qing Ye Liu ◽  
Zhi Liang Jiang

In pH 6.5 Na2HPO4-NaH2PO4 buffer solution and in the presence of stable reagent PEG10000 and aggregation reagent NaCl, nanosilvers were aggregated to form stable aggregated-nanosilvers (ANS). The molecular probe of 4-mercaptopyridine (MP) adsorbed on the surface of ANS to form MP-ANS conjugates that produce strongest surface-enhanced resonance Raman scattering (SERRS) peak at 1097 cm-1. When Au(III) was added, the SERRS intensity at 1097 cm-1 decreased. The decreased SERRS intensity was linear to Au(III) concentration in the range of 5-50 ×10-10 mol/L, with a detection limit of 2.0×10-10 mol/L Au(III).


2020 ◽  
Vol 1 (2) ◽  
pp. 146-152 ◽  
Author(s):  
Satheeshkumar Elumalai ◽  
John R. Lombardi ◽  
Masahiro Yoshimura

The resonance Raman signal enhancement of crystal violet dyes onto the two-dimensional MXene–Ti3C2Tx film, so called MXenes-enhanced resonance Raman scattering (MERRS), is reported with a calculated enhancement factor of 3.42 × 109.


2013 ◽  
Vol 319 ◽  
pp. 157-160 ◽  
Author(s):  
Xin Hui Zhang ◽  
Kun Li ◽  
Le Ning Hu ◽  
Ai Hui Liang ◽  
Zhi Liang Jiang

In pH 6.6 Na2HPO4-citric acid buffer solution and in the presence of KCl, the nanosilver-labeled rabbit anti-hCG (Ag-RAhCG) was aggregated un-specifically to the aggregations. Upon addition of rhodamine 6G (RhG) molecular probe, it adsorb on the surface of Ag-RAhCG aggregations that exhibited the strongest surface-enhnaced resonance Raman scattering (SERRS) peak at 613 cm-1. In the optimal condition, the decreased SERRS intensity responds linearly with the concentration of hCG over 0.05-1.75 µg/mL. Based on this, a new and simple SERRS method has been proposed for the determination of hCG in serum samples, with satisfactory results.


Plasmonics ◽  
2012 ◽  
Vol 8 (2) ◽  
pp. 803-810 ◽  
Author(s):  
Zhiliang Jiang ◽  
Dongmei Yao ◽  
Guiqing Wen ◽  
Tingsheng Li ◽  
Bin Chen ◽  
...  

2006 ◽  
Vol 789 (1-3) ◽  
pp. 59-70 ◽  
Author(s):  
Prokopis C. Andrikopoulos ◽  
Karen M. McCarney ◽  
David R. Armstrong ◽  
Rachael E. Littleford ◽  
Duncan Graham ◽  
...  

ChemInform ◽  
2010 ◽  
Vol 29 (40) ◽  
pp. no-no
Author(s):  
D. GRAHAM ◽  
C. MCLAUGHLIN ◽  
G. MCANALLY ◽  
J. C. JONES ◽  
P. C. WHITE ◽  
...  

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