3D/4D Strain Mapping Using In Situ X-Ray Microtomography

2011 ◽  
Vol 70 ◽  
pp. 249-254 ◽  
Author(s):  
Hiroyuki Toda ◽  
Kentaro Uesugi ◽  
Yoshio Suzuki ◽  
Masakazu Kobayashi

X-ray microtomography (XMT) has been utilized for the in-situ observation of various structural materials under external disturbance such as loading. In-situ XMT provides a unique possibility to access the three-dimensional (3D) character of internal microstructure and its time evolution behaviours non-destructively, thereby enabling advanced techniques for measuring local strain distribution. Local strain mapping is readily enabled by processing such high-resolution tomographic images either by the particle tracking technique or the digital image correlation technique. Procedures for tracking microstructural features which have been developed by the authors, have been applied to analyse localised deformation and damage evolution in a material. Typically several tens of thousands of microstructural features, such as particles and pores, are tracked in a tomographic specimen (0.2 - 0.3 mm3in volume). When a sufficient number of microstructural features is dispersed in 3D space, the Delaunay tessellation algorithm is used to obtain local strain distribution. With these techniques, 3D strain fields can be measured with reasonable accuracy. Even local crack driving forces, such as local variations in the stress intensity factor, crack tip opening displacement and J integral along a crack front line, can be measured from discrete crack tip displacement fields.

2011 ◽  
Vol 6 (11) ◽  
pp. C11007-C11007 ◽  
Author(s):  
Tomáš Doktor ◽  
Ondřej Jiroušek ◽  
Daniel Kytýř ◽  
Petr Zlámal ◽  
Ivan Jandejsek

Author(s):  
Xinnan Wang ◽  
Peng Cui ◽  
X. W. Tangpong

In this study, the mechanical properties of multi-walled carbon nanotubes (MWCNTs) reinforced epoxy nanocomposite were measured with the custom-built micro/nano three point bending tester mounted on an atomic force microscope (AFM). With in-situ observation of the AFM, the movement of an individual MWCNT on the sample surface was traced, captured, and quantified using the image correlation technique. The Halpin-Tsai and Hui-shia models were applied and compared with the experimental data. Results showed that the elastic modulus from the experiment is much lower than the predicted values from the two models. Detailed mechanical deformation behavior and MWCNT reinforcement mechanism were discussed.


2014 ◽  
Vol 891-892 ◽  
pp. 301-306 ◽  
Author(s):  
Angelika Brueckner-Foit ◽  
Pascal Pitz ◽  
Frank Zeismann ◽  
Lisa Zellmer

Hard phases such as martensite regions affect micro-crack extension by blocking the plastic zone ahead of the crack tip, but also by changing the crack opening which can be taken as loading quantity for cracks. This paper deals with the measurement of crack opening for microcracks in a ferrite/martensite dual phase steel. The methods used are in-situ testing in the SEM, X-ray tomography, and digital image correlation. It was found that martensite regions affect the relative displacement of the crack phases both at the crack tip and in the crack wake.


2018 ◽  
Vol 165 ◽  
pp. 06004
Author(s):  
Zhang Wei ◽  
Zhou Daoqing ◽  
Cai Liang

The plastic deformation ahead of crack tip is of great significance to analysis of the fatigue crack growth behaviour. Using the in-situ microscopy experiment technique, the variation of strain field in the vicinity of crack tip is investigated within load cycles at the small time scale. The contours of plastic zones are measured through the in-situ observation and digital image correlation (DIC). Finite element method (FEM) is also used to simulate the plasticity ahead of the crack tip. Furthermore, the numerical studies are extended to the single overload case to analyse the effect of large plastic zone on the subsequent crack growth. The evolution of residual stress is extracted by FEM simulation to explore the influence of plastic deformation before, during and after the single overload applied on the following crack propagation. Based on the FEM analysis, a model is proposed to approximate the size of the overload effect zone. Finally, some experimental data and numerical simulations are employed to validate this model.


1993 ◽  
Vol 308 ◽  
Author(s):  
Paul R. Besser ◽  
Thomas N. Marieb ◽  
John C. Bravman

ABSTRACTStrain relaxation in passivated Al-0.5% Cu lines was measured using X-ray diffraction coupled with in-situ observation of the formation and growth of stress induced voids. Samples of 1 μm thick Al-0.5% Cu lines passivated with Si3N4 were heated to 380ºC, then cooled and held at 150ºC. During the test, principal strains along the length, width, and height of the line were determined using a grazing incidence x-ray geometry. From these measurements the hydrostatic strain in the metal was calculated and strain relaxation was observed. The thermal cycle was duplicated in a high voltage scanning transmission electron microscope equipped with a backscattered electron detector. The 1.25 μm wide lines were seen to have initial stress voids. Upon heating these voids reduced in size until no longer observable. Once the samples were cooled to 150ºC, voids reappeared and grew. The measured strain relaxation is discussed in terms of void and θ-phase (Al2Cu) formation.


2021 ◽  
pp. 2100201
Author(s):  
Philipp Jordt ◽  
Stjepan B. Hrkac ◽  
Jorit Gröttrup ◽  
Anton Davydok ◽  
Christina Krywka ◽  
...  

ChemInform ◽  
2006 ◽  
Vol 37 (12) ◽  
Author(s):  
Katsuhiro Kobayashi ◽  
Tadashi Hata ◽  
Hiroshi Fukuhara ◽  
Yuji Ohashi
Keyword(s):  

2011 ◽  
Vol 59 (5) ◽  
pp. 1995-2008 ◽  
Author(s):  
H. Toda ◽  
E. Maire ◽  
S. Yamauchi ◽  
H. Tsuruta ◽  
T. Hiramatsu ◽  
...  

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