Experimental Study on Extraction of Scandium from Hydrochloride Acid Leaching Liquid in TBP

2013 ◽  
Vol 807-809 ◽  
pp. 2440-2443
Author(s):  
Gui Fang Zhang ◽  
Peng Yan ◽  
Qing Rong Yang
Keyword(s):  
Hydrochloric Acid ◽  
Acid Solution ◽  
Hydrochloric Acid Solution ◽  
Yunnan Province ◽  
Mixing Time ◽  
Acid Leaching ◽  
Phase Ratio ◽  
Optimal Conditions ◽  
Impurity Composition ◽  
Leaching Experiment

The scandium concentrate used in the leaching experiment was obtained from the rare earth ore containing scandium in Yunnan Province, the sample used in experiment is leaching liquid containing scandium which the content of scandium is 3.6g/t, with complex impurity composition. The main influencing factors of extraction in hydrochloric acid solution were acidity, mixing time, phase ratio etc. and the condition experiments about these factors were conducted. The results show that extraction of scandium from the hydrochloric acid solution in TBP is feasible. The optimal conditions are that pH of the solution is 1.26, dosage of TBP is 5% of the solution, dosage of kerosene is 10% of TBP, mixing time is 3 min, phase ratio is 1:10, washing time is 2, the oscillating time of stripping is 1~2 min and the stripping rate reach 99.89%.

A 35Cl magnetic resonance study of chloride exchange on indium(III) and thallium(III) in aqueous hydrochloric acid solution

1975 ◽  
Vol 28 (9) ◽  
pp. 1901 ◽  
Author(s):  
SF Lincoln ◽  
AC Sandercock ◽  
DR Stranks
Keyword(s):  
Exchange Rate ◽  
Magnetic Resonance ◽  
Hydrochloric Acid ◽  
Acid Solution ◽  
Hydrochloric Acid Solution ◽  
Magnetic Resonance Study ◽  
Aqueous Hydrochloric Acid ◽  
Chloride Exchange ◽  
Lower Limits ◽  
Aqueous Hydrochloric Acid Solution

The parameters describing chloride exchange on indium(III), determined by 35Cl N.M.R., are: k(298 K)= (8.8�0+4) x 106 s-1, ΔH? = 45.7�2.3 kJ mol-1 and ΔS? = 42�8 J mol-1 K-1; and k(298 K)= (2.0�0.1)x106 s-1, ΔH? = 37.7�1.9 kJ mol-1, and ΔS? = 3�6 J mol-1 K-1 in 10.95M and 7.00M aqueous hydrochloric acid respectively, calculated from the observed exchange rate kex4[InCl4(H2O)2-].��� For thallium(III) lower limits of kex(219 K) = 1.6 x 106 s-1 and 1.3 x 106 s-1 were obtained in 10.95M and 7.00M aqueous hydrochloric acid, respectively, where [TlCl6]3- is assumed to be the exchanging species.

scholarly journals Investigation of the corrosion inhibition of carbon steel in hydrochloric acid solution by using ginger roots extract

RSC Advances ◽  
2017 ◽  
Vol 7 (40) ◽  
pp. 24576-24588 ◽  
Author(s):  
H. S. Gadow ◽  
M. M. Motawea
Keyword(s):  
Carbon Steel ◽  
Hydrochloric Acid ◽  
Acid Solution ◽  
Corrosion Inhibition ◽  
Hydrochloric Acid Solution ◽  
Adsorption Behavior ◽  
Different Temperatures ◽  
Hcl Solution

The inhibitive effect and adsorption behavior of ginger roots extract (GRE) on the corrosion of carbon steel in 1.0 M HCl solution at different temperatures were investigated.

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