Crystal Structure of Biammonium Hexamolybdonickelate (II) Hydrate, (NH4)2(NiMo6O24)(H3O)6

2013 ◽  
Vol 834-836 ◽  
pp. 485-489
Author(s):  
Hai Xing Liu ◽  
Qing Liu ◽  
Quan Hua Fan ◽  
Xiao Ping Zhang ◽  
Lin Tong Wang ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Metal Complex ◽  
Title Compound ◽  
Hydrothermal Reaction ◽  
Ammonium Cation ◽  
Water Molecules ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions

A novel Ni metal complex H26Mo6N2NiO30has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. H26Mo6N2NiO30, Monoclinic, P2(1)/c. a = 11.3487(14) Å, b = 11.0823(13) Å, c = 11.9350(16) Å. alpha=gamma= 90°. beta= 108.542(2)°. V= 1423.1(3) Å3. It is also striking that the structure of title compound exhibits extensive hydrogen-bonding interactions among water molecules, ammonium cation, and oxygen atoms in the heteropolyanion.

Study on a Structure of 2,6-Pyridine-Dicarboxylic Acid Europium Quarthydrate

2013 ◽  
Vol 834-836 ◽  
pp. 490-493
Author(s):  
Hai Xing Liu ◽  
Qing Liu ◽  
Yang Xu ◽  
Ting Ting Huang ◽  
Lin Tong Wang ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Metal Complex ◽  
Hydrothermal Reaction ◽  
Crystal Packing ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
Pyridine Dicarboxylic Acid ◽  
The Eu

A novel Eu metal complex C14H19EuN2O14has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Eu atom is nine-coordinated by two N atom and seven O atoms. The crystal packing is stabilized by O-H...O hydrogen bonding interactions

Study on a Structure of 2,6-Pyridine-Dicarboxylic Acid Mn, Mn2(C7H3NO4)24H2O

2013 ◽  
Vol 785-786 ◽  
pp. 428-431 ◽  
Author(s):  
Hai Xing Liu ◽  
Qing Hua Zhang ◽  
Zhang Xue Yu ◽  
Xiao Ping Zhang ◽  
Yang Xu ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Metal Complex ◽  
Dicarboxylic Acid ◽  
Hydrothermal Reaction ◽  
Crystal Packing ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
Pyridine Dicarboxylic Acid

A novel Mn metal complex C14H14Mn2N2O12 has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Mn atom is six-coordinated by one N atom and four O atoms. The Mn-Mn bond is existent. The crystal packing is stabilized by O-H...O hydrogen bonding interactions.

Study on Novel Structure of Praseodymium Complex, C5H13O11Pr

2013 ◽  
Vol 834-836 ◽  
pp. 515-518
Author(s):  
Hai Xing Liu ◽  
Qing Liu ◽  
Ting Ting Huang ◽  
Yang Xu ◽  
Lin Tong Wang ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Single Crystal ◽  
Hydrothermal Reaction ◽  
Crystal Packing ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
Novel Structure ◽  
Praseodymium Complex

A novel praseodymium complex C5H13O11Pr has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Pr1 atom is nine coordinated by nine O atoms. The crystal packing is stabilized by O-H...O hydrogen bonding interactions.

Synthesis of Glycolic and Oxalic Acid Europium: [Eu (C3 H6O9)] ·2(H2O)

2012 ◽  
Vol 554-556 ◽  
pp. 792-795
Author(s):  
Hai Xing Liu ◽  
Jing Wang ◽  
Fang Fang Jian ◽  
Hui Juan Yue ◽  
Guang Zeng ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Oxalic Acid ◽  
Single Crystal ◽  
Hydrothermal Reaction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
The Eu

A new Eu complex [Eu (C3O9H6)] ·2(H2O) has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Eu atom is coordinated by eight O atoms. The molecular is antisymmetric structure by the C3-C3 axis. It is striking that the structure of the complex exhibits extensive O-H…O hydrogen-bonding interactions.

Study on a Novel Structure of Yttrium Complex, C4H10O10Y

2013 ◽  
Vol 785-786 ◽  
pp. 424-427
Author(s):  
Hai Xing Liu ◽  
Qing Hua Zhang ◽  
Zhang Xue Yu ◽  
Quan Hua Fan ◽  
Ting Ting Huang ◽  
...  
Keyword(s):  
Molecular Structure ◽  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Single Crystal ◽  
Hydrothermal Reaction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
Novel Structure

The Y complex C4H10O10Y has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Y atom is coordinated by nine O atoms. The molecular structure stabilized by the O-H…O hydrogen-bonding interactions.

scholarly journals Study on novel structure of tris-(4,4′-dimethyl-2,2′-dipyridyl) Nickel salicylic acid boric acid, Ni(C12H12N2)3●(C7H5O3)2●(H3BO3)

2021 ◽  
Vol 252 ◽  
pp. 02069
Author(s):  
Xiaoyan Ren ◽  
Haixing Liu ◽  
Yanfang Huo
Keyword(s):  
Molecular Structure ◽  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Salicylic Acid ◽  
Hydrothermal Reaction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
Novel Structure ◽  
Novel Complex

A novel complex Ni(C12H12N2)3●(C7H5O3)2●(H3BO3) has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. Triclinic, P-1. a= 12.5380(13) Å, b = 13.0100(15) Å, c = 15.1490(18) Å, α= 102.760(3)°, β= 94.480(2)°, γ= 94.540(2)°. V=2390.9(5) Å3. Z=2. R1 =0.0661, wR2 = 0.2128, T=293(2) K. The Ni atom is coordinated by six N atoms from three 4,4′-dimethyl-2,2′-dipyridyl molecular. The molecular structure stabilized by the O-H…O hydrogen-bonding interactions.

Study on a Novel Structure of Europium Complex, C4H10EuO10

2014 ◽  
Vol 488-489 ◽  
pp. 252-255
Author(s):  
Hai Xing Liu ◽  
Qing Liu ◽  
Huan Mei Guo ◽  
Quan Hua Fan ◽  
Xiao Ping Zhang ◽  
...  
Keyword(s):  
Molecular Structure ◽  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Hydrothermal Reaction ◽  
Europium Complex ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
Novel Structure ◽  
The Eu

The Eu complex C4H10EuO10has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Eu atom is coordinated by nine O atoms. The molecular structure stabilized by the O-H…O hydrogen-bonding interactions.

Crystal structure of dicadmium(II) ethylenediphosphinetetraacetate octahydrate

1991 ◽  
Vol 56 (7) ◽  
pp. 1454-1460 ◽  
Author(s):  
Jaroslav Podlaha ◽  
Jana Podlahová
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Single Crystal ◽  
Diffraction Data ◽  
Title Compound ◽  
Water Molecules ◽  
X Ray Diffraction ◽  
Coordination Polyhedra ◽  
X Ray ◽  
Carboxylate Groups

The crystal structure of the title compound containing a phosphorus analogue of EDTA as the ligand was determined from single-crystal X-ray diffraction data and refined to R = 0.028 for 1 920 observed reflections. The crystals are monocyclic, space group P21/c,a = 8.6169(8), b = 16.0539(9), c = 8.2504(6)Å, β = 103.458(7)° and Z = 2. The structure is completely different from that of the nitrogen prototype, [CdEDTA]2-. It consists of double-stranded polymeric layers which are composed of metal coordination polyhedra linked by μ6-hexadentate ligands; the layers lie parallel to the bc plane and are joined along the a axis through hydrogen bonding donated by water molecules. Because of steric requirements of phosphorus, the coordination polyhedron around Cd is greatly distorted and can best be described as a 5 + 3 type. One P atom, two oxygen atoms from two monodentate carboxylate groups and two water molecules form an approximate trigonal bipyramid and further three more remote carboxylate oxygens complete the arrangement, resulting in an O7P distorted bicapped trigonal prism.

Study on a Structure of 2,6-pyridine-dicarboxylic Acid Cobalt Calcium Hexahydrate

2013 ◽  
Vol 739 ◽  
pp. 30-33
Author(s):  
Hai Xing Liu ◽  
Jing Zhong Xiao ◽  
Huan Mei Guo ◽  
Qing Hua Zhang ◽  
Zhang Xue Yu ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Dicarboxylic Acid ◽  
Hydrothermal Reaction ◽  
Crystal Packing ◽  
X Ray Diffraction ◽  
X Ray ◽  
Hydrogen Bonding Interactions ◽  
Pyridinedicarboxylic Acid ◽  
Pyridine Dicarboxylic Acid

The complex C28H32CaCoN4O24has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Co atom is six-coordinated by two N atoms, four O atoms from two 2,6-pyridinedicarboxylic acid. The Ca atom is eight-coordinated by two N atoms, six O atoms from two 2,6-pyridinedicarboxylic acid and two water molecular. The crystal packing is stabilized by O-H...O hydrogen bonding interactions.

Study on Novel Structure of Gadolinium Complex: Gd (C3 H6O9)

2012 ◽  
Vol 557-559 ◽  
pp. 401-404
Author(s):  
Hai Xing Liu ◽  
Li Mei Wan ◽  
Qing Zhi Pan ◽  
Hui Juan Yue ◽  
Guang Zeng ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonding ◽  
Layered Structure ◽  
Hydrothermal Reaction ◽  
Two Dimensional ◽  
X Ray Diffraction ◽  
X Ray ◽  
Gadolinium Complex ◽  
Hydrogen Bonding Interactions ◽  
Novel Structure

A novel Gadolinium complex Gd (C3O9H6) has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. The Gd atom is coordinated by sixteen O atoms. The two-dimensional layered structure is formed and exhibits extensive O-H…O hydrogen-bonding interactions.

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