Studies on the Microstructure of Pure and Doped Anatase TiO2 Nanoparticles by SAXS

Materials Science Forum ◽

10.4028/www.scientific.net/msf.743-744.831 ◽

2013 ◽

Vol 743-744 ◽

pp. 831-836 ◽

Author(s):

Wei Mei Shi ◽

Xiao Jun Dai ◽

Guang Cheng Yang ◽

Yao Xu ◽

Yi Liu

Keyword(s):

Photocatalytic Activity ◽

Synchrotron Radiation ◽

Hydrothermal Method ◽

Rough Surface ◽

Small Angle ◽

Sol Gel ◽

Negative Deviation ◽

X Ray ◽

X Ray Scattering ◽

Fractal Properties

Pure TiO2, Ce-doped and Ce/Si-codoped TiO2 nanoparticles with different Ce contents were synthesized by using a sol-gel-hydrothermal method. The as-synthesized samples were annealed at 400 °C. Their crystallization was investigated by Raman spectroscope. The result showed that Ce-doping and Ce-Si codoping decreased the crystallization. The interfacial and fractal properties were investigated by synchrotron radiation small angle X-ray scattering (SAXS). The results indicated that Ce-doping induced the Porod negative deviation, and the fractal properties showed TiO2 nanoparticles codoped by Ce-Si were rougher than these of the pure TiO2 and Ce-doped TiO2. This rough surface of the nanoparticles was helpful to improve the photocatalytic activity.

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Precise and nondestructive characterization of a ‘buried’ nanostructure in a polymer thin film using synchrotron radiation ultra-small angle X-ray scattering

Polymer Journal ◽

10.1038/pj.2012.133 ◽

2012 ◽

Vol 45 (3) ◽

pp. 307-312 ◽

Author(s):

Takamichi Shinohara ◽

Tomoko Shirahase ◽

Daiki Murakami ◽

Taiki Hoshino ◽

Moriya Kikuchi ◽

...

Keyword(s):

Thin Film ◽

Synchrotron Radiation ◽

Small Angle ◽

Polymer Thin Film ◽

X Ray ◽

X Ray Scattering ◽

Nondestructive Characterization ◽

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The Significance of Solutions Obtained from Ill-Posed Systems of Linear Equations Constituted by Synchrotron Radiation Based Anomalous Small-Angle X-Ray Scattering

Advances in Linear Algebra &amp Matrix Theory ◽

10.4236/alamt.2018.81007 ◽

2018 ◽

Vol 08 (01) ◽

pp. 64-86 ◽

Author(s):

Günter Johannes Goerigk

Keyword(s):

Synchrotron Radiation ◽

Small Angle ◽

Linear Equations ◽

X Ray ◽

X Ray Scattering ◽

Systems Of Linear Equations ◽

Ill Posed ◽

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Nucleation of atomic-layer-deposited HfO2 films, and evolution of their microstructure, studied by grazing incidence small angle x-ray scattering using synchrotron radiation

Applied Physics Letters ◽

10.1063/1.2164417 ◽

2006 ◽

Vol 88 (3) ◽

pp. 032907 ◽

Author(s):

M. L. Green ◽

A. J. Allen ◽

X. Li ◽

J. Wang ◽

J. Ilavsky ◽

...

Keyword(s):

Synchrotron Radiation ◽

Small Angle ◽

Atomic Layer ◽

Grazing Incidence ◽

X Ray ◽

X Ray Scattering ◽

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Upgrade of the BioMUR beamline at the Kurchatov synchrotron radiation source for serial small-angle X-ray scattering experiments in solutions

Nuclear Instruments and Methods in Physics Research Section A Accelerators Spectrometers Detectors and Associated Equipment ◽

10.1016/j.nima.2021.166170 ◽

2021 ◽

pp. 166170

Author(s):

G.S. Peters ◽

Yu.A. Gaponov ◽

P.V. Konarev ◽

M.A. Marchenkova ◽

K.B. Ilina ◽

...

Keyword(s):

Synchrotron Radiation ◽

Small Angle ◽

Radiation Source ◽

Synchrotron Radiation Source ◽

X Ray ◽

X Ray Scattering ◽

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Small Angle X-Ray Scattering (SAXS) with Synchrotron Radiation Sources

Synchrotron Radiation ◽

10.1007/978-3-642-55315-8_11 ◽

2014 ◽

pp. 337-359

Author(s):

Stefano Polizzi ◽

Francesco Spinozzi

Keyword(s):

Synchrotron Radiation ◽

Small Angle ◽

X Ray ◽

X Ray Scattering ◽

Radiation Sources ◽

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Small-angle X-ray scattering investigation of aging behavior of Al-Cu-Mg-Ag alloys using synchrotron radiation

Rare Metals ◽

10.1007/s12598-012-0553-0 ◽

2012 ◽

Vol 31 (6) ◽

pp. 537-540

Author(s):

Jianbo Zhang ◽

Yongan Zhang ◽

Baohong Zhu ◽

Ruiqing Liu ◽

Zhihui Li ◽

...

Keyword(s):

Synchrotron Radiation ◽

Small Angle ◽

Aging Behavior ◽

X Ray ◽

X Ray Scattering ◽

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Time-resolved small angle X-ray scattering study of sol–gel precursor solutions of lead zirconate titanate and zirconia

Journal of Colloid and Interface Science ◽

10.1016/j.jcis.2011.12.033 ◽

2012 ◽

Vol 369 (1) ◽

pp. 184-192 ◽

Author(s):

Tomasz M. Stawski ◽

Rogier Besselink ◽

Sjoerd A. Veldhuis ◽

Hessel L. Castricum ◽

Dave H.A. Blank ◽

...

Keyword(s):

Lead Zirconate Titanate ◽

Small Angle ◽

Sol Gel ◽

Lead Zirconate ◽

Time Resolved ◽

X Ray ◽

X Ray Scattering ◽

Zirconate Titanate ◽

Scattering Study ◽

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Unfolding of dimeric creatine kinase in urea and guanidine hydrochloride as measured using small angle X-ray scattering with synchrotron radiation

FEBS Letters ◽

10.1016/s0014-5793(97)01120-4 ◽

1997 ◽

Vol 415 (2) ◽

pp. 183-185 ◽

Author(s):

Jun-Mei Zhou ◽

Ying-Xin Fan ◽

Hiroshi Kihara ◽

Kazumoto Kimura ◽

Yoshiyuki Amemiya

Keyword(s):

Creatine Kinase ◽

Synchrotron Radiation ◽

Small Angle ◽

Guanidine Hydrochloride ◽

X Ray ◽

X Ray Scattering ◽

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Determination of the temperature and time dependence of the absolute small-angle X-ray scattering intensity of partially crystalline polymers employing synchrotron radiation

Polymer ◽

10.1016/0032-3861(89)90316-9 ◽

1989 ◽

Vol 30 (9) ◽

pp. 1582-1590 ◽

Author(s):

R. Gehrke ◽

C. Riekel ◽

H.G. Zachmann

Keyword(s):

Synchrotron Radiation ◽

Time Dependence ◽

Small Angle ◽

Scattering Intensity ◽

X Ray ◽

Crystalline Polymers ◽

X Ray Scattering ◽

The Absolute ◽

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X-ray reflectivity, diffraction and grazing incidence small angle X-ray scattering as complementary methods in the microstructural study of sol–gel zirconia thin films

Thin Solid Films ◽

10.1016/j.tsf.2005.08.335 ◽

2006 ◽

Vol 495 (1-2) ◽

pp. 224-231 ◽

Author(s):

P. Lenormand ◽

A. Lecomte ◽

D. Babonneau ◽

A. Dauger

Keyword(s):

Small Angle ◽

Sol Gel ◽

Grazing Incidence ◽

Microstructural Study ◽

X Ray ◽

Complementary Methods ◽

X Ray Scattering ◽

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