scholarly journals Determination of iodine content in milk and food supplements by inductively coupled plasma mass spectrometry (ICP-MS)

Author(s):  
Chien Dinh Viet ◽  
Hieu Pham Cong ◽  
Thoa Nguyen Bao ◽  
Chau Nguyen Minh ◽  
Ha Le Van ◽  
...  

The determination of iodine in milk and food supplements by inductively coupled plasma mass spectrometry (ICP-MS) was investigated. Several parameters of the equipment were optimized automatically such as power of radio frequency, nebulizer gas, and voltage of ion lens. Iodine was extracted from samples by using 2% HNO3 with ultrasonic at 80ºC. Sample solutions were adjusted to the pH of 9÷10 by using ammonium hydroxide, and then filtered by using a 0.45 µm membrane before being analyzed by means of ICP-MS. The method has good repeatability and high recovery efficiency that are suitable for the determination of iodine in milk and food supplements.

2018 ◽  
Vol 33 (12) ◽  
pp. 2143-2152 ◽  
Author(s):  
Zhian Bao ◽  
Chunlei Zong ◽  
Lu Chen ◽  
Danbo Lei ◽  
Kaiyun Chen ◽  
...  

In this study, Pb isotope ratios in ferromanganese nodules were determined with good repeatability and minimum laboratory bias using laser ablation multi-collector inductively coupled plasma mass spectrometry (LA-MC-ICP-MS).


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