Brisk Method for Fractionating and Separating Bio-Crude Oil

Flame Ionisation ◽

A new approach for the analysis of bio-crude oils (BCOs) has been qualitatively explored. The analytical scheme is based on the fractionation of BCO through precipitation in water, freeze-drying, solid phase extraction (SPE) and combinations of analytical techniques for the analysis of fractions. Monomeric components in BCO were characterised using gas chromatography coupled with mass spectrometer and flame ionisation detector (GC-MS/FID). The molecular mass distribution of oligomers was determined using gel permeation chromatography (GPC). The fractionation procedure appeared to have succeeded to a large extent as evident in the detection of various components along their expected fraction in the GC-MS/FID analysis. However, a quantitative analysis of the multiple components in different fractions appeared difficult owing to the loss of many volatile fractions through the fractionation procedure. And less than 7 wt. % of the sugar-related components in the acetylated polar SPE fraction were identified.

Rapid monitoring of carvacrol in plants and herbal medicines using matrix solid-phase dispersion and gas chromatography flame ionisation detector

Natural Product Research ◽

10.1080/14786419.2014.980247 ◽

2014 ◽

Vol 29 (7) ◽

pp. 621-627 ◽

Cited By ~ 14

Author(s):

Marzieh Rashidipour ◽

Rouhollah Heydari ◽

Alireza Feizbakhsh ◽

Payman Hashemi

Keyword(s):

Gas Chromatography ◽

Solid Phase ◽

Herbal Medicines ◽

Matrix Solid Phase Dispersion ◽

Phase Dispersion ◽

Rapid Monitoring ◽

Flame Ionisation ◽

An efficient method for the simultaneous determination of furan, 2-methylfuran and 2-pentylfuran in fruit juices by headspace solid phase microextraction and gas chromatography–flame ionisation detector

Food Chemistry ◽

10.1016/j.foodchem.2015.06.100 ◽

2016 ◽

Vol 192 ◽

pp. 9-14 ◽

Cited By ~ 22

Author(s):

Gaofei Hu ◽

Yan Zhu ◽

Marta Hernandez ◽

Tatiana Koutchma ◽

Suqin Shao

Keyword(s):

Gas Chromatography ◽

Simultaneous Determination ◽

Efficient Method ◽

Solid Phase Microextraction ◽

Solid Phase ◽

Headspace Solid Phase Microextraction ◽

Flame Ionisation ◽

Determination of furanic compounds in mopane worms, corn, and peanuts using headspace solid-phase microextraction with gas chromatography-flame ionisation detector

Food Chemistry ◽

10.1016/j.foodchem.2021.130944 ◽

2021 ◽

pp. 130944

Author(s):

Nonkululeko S. Masite ◽

Somandla Ncube ◽

Fanyana M. Mtunzi ◽

Lawrence M. Madikizela ◽

Vusumzi E. Pakade

Keyword(s):

Gas Chromatography ◽

Solid Phase Microextraction ◽

Solid Phase ◽

Headspace Solid Phase Microextraction ◽

Furanic Compounds ◽

Flame Ionisation ◽

Determination of furan in food samples using two solid phase microextraction fibers based on sol–gel technique with gas chromatography–flame ionisation detector

Food Chemistry ◽

10.1016/j.foodchem.2011.09.019 ◽

2012 ◽

Vol 131 (2) ◽

pp. 698-704 ◽

Cited By ~ 34

Author(s):

Ali Sarafraz-Yazdi ◽

Maryam Abbasian ◽

Amirhassan Amiri

Keyword(s):

Gas Chromatography ◽

Solid Phase Microextraction ◽

Solid Phase ◽

Sol Gel ◽

Food Samples ◽

Gel Technique ◽

Flame Ionisation ◽

Using a flame ionisation detector to measure the rate and duration of pyrolysis of a biomass particle

Combustion and Flame ◽

10.1016/j.combustflame.2021.111438 ◽

2021 ◽

Vol 230 ◽

pp. 111438

Author(s):

Andras Volford ◽

Thomas Redko ◽

Ewa J. Marek ◽

Zach.W.M. Bond ◽

Allan N. Hayhurst

Keyword(s):

Flame Ionisation ◽

Investigation of cultivated lavender (Lavandula officinalis L.) extraction and its extracts

Chemical Industry and Chemical Engineering Quarterly ◽

10.2298/ciceq120715103n ◽

2014 ◽

Vol 20 (1) ◽

pp. 71-86 ◽

Cited By ~ 13

Author(s):

Vesna Nadjalin ◽

Zika Lepojevic ◽

Mihailo Ristic ◽

Jelena Vladic ◽

Branislava Nikolovski ◽

...

Keyword(s):

Gas Chromatography ◽

Essential Oil ◽

Experimental Results ◽

Main Components ◽

Lavandula Officinalis ◽

Physical And Chemical ◽

Kinetics Of ◽

Flame Ionisation ◽

In this study essential oil content was determined in lavender flowers and leaves by hydrodistillation. Physical and chemical characteristics of the isolated oils were determined. By using CO2 in supercritical state the extraction of lavender flowers was performed with a selected solvent flow under isothermal and isobaric conditions. By the usage of gas chromatography in combination with mass spectrometry (GC/MS) and gas chromatography with flame ionisation detector (GC/FID) the qualitative and quantitative analysis of the obtained essential oil and supercritical extracts (SFE) was carried out. Also, the analysis of individual SFE extracts obtained during different extraction times was performed. It turned out that the main components of the analysed samples were linalool, linalool acetate, lavandulol, caryophyllene oxide, lavandulyl acetate, terpinen-4-ol and others. Two proposed models were used for modelling the extraction system lavender flower - supercritical CO2 on the basis of experimental results obtained by examining the extraction kinetics of this system. The applied models fitted well with the experimental results.