Orientation Dependence of the Substructure Characteristics in a Ni-30%Fe Austenitic Alloy Deformed in Hot Torsion

The present work examines the microstructure and texture evolution in a Ni-30wt.%Fe austenitic model alloy deformed in torsion at 1000 °C, with a particular emphasis on the orientation dependence of the substructure characteristics within the deformed original grains. Texture of these grains was principally consistent with that expected for simple shear and comprised the main A, B and C components. The deformation substructure within the main texture component grains was characterised by “organised” arrays of parallel microbands with systematically alternating misorientations, locally accompanied by micro-shear bands within the C grains. With increasing strain, the mean subgrain size gradually decreased and the mean misorientation angle concurrently increased towards the saturation. The stored deformation energy within the main texture component grains was principally consistent with the respective Taylor factor values. The microband boundaries corresponded to the expected single slip {111} plane for the A oriented grains while these boundaries for the C oriented grains represented a variety of planes even for a single grain.

Orientation Evolution during Equal Angular Channel Extrusion of Copper Single Crystal

The orientation evolution in Copper single crystal during ECAE (in Route C) has been investigated experimentally for 90° die angle by X-ray diffraction and TEM-OIM. It is shown that after the previous three passes of ECAE, orientation evolutes with similar mechanism to the simple shear deformation. The grain subdivision occurs with the appearance of many low angle grain boundaries. After four times extrusions the ED of the samples remains stable, their ND rotates around the ED by about 20°. After five times extrusions the main texture component remains stable.

Quantitative texture analysis with the HIPPO neutron TOF diffractometer

One of the design goals of the neutron time-of-flight (TOF) diffractometer HIPPO (High Pressure–Preferred Orientation) at LANSCE (Los Alamos Neutron Science Center) was efficient quantitative texture analysis. In this paper, the effects of the HIPPO detector geometry and layout on texture analysis, particularly the shape and dimensions of the detector panels, are investigated in detail. An equal-channel angular-pressed (ECAP) aluminium sample with a strong texture was used to determine the methodological limitations of various methods of quantitative texture analysis. Several algorithms for extracting the orientation distribution function (ODF) from the TOF spectra are compared: discrete orientations at arbitrary positions, harmonic methods in Rietveld codes (MAUD and GSAS) and discrete methods in MAUD. Because of the detector geometry, the sharpest texture peaks that can be represented are 12–15° in width, resulting in an optimal texture resolution of 25–30°. Due to the limited resolution and incomplete pole-figure coverage, harmonic expansions beyond L = 12 (where L is the maximum degree of the harmonic expansion) introduce subsidiary oscillations, which are consistently identified as artifacts. Only discrete methods provide a quantitative representation of the texture. Harmonic methods are adequate for a qualitative description of the main texture component. The results of the analysis establish HIPPO as an efficient instrument to determine preferred orientations in relatively short measuring times.