Tem Study of Nanostructured Magnesium Aluminate Spinel Phase Formation

Author(s):  
Jafar F. Al-Sharab ◽  
James Bentley ◽  
Amit Singhal ◽  
Ganesh Skandan ◽  
Frederic Cosandey
2012 ◽  
Vol 512-515 ◽  
pp. 600-603 ◽  
Author(s):  
Jiang Feng Tong ◽  
Da Ming Chen

In this paper, a fine pure Magnesium aluminate spinel powder was synesised by Gel solid reaction,using Al(NO3)36H2O and Mg(NO3)26H2O as raw materials under given condition. The precursor was formed by polymer gelling.The phase changed according to heating temperatures from 700°C to 900°C.The single phase of Magnesium aluminate spinel was obtained by calcining the precursor at temperatures higher than 900°C. The phase changing process and relationship among calcination parameters, phase composition and image of particle are studied to determine the optimal conditions for the synthesis of fine Magnesium aluminate spinel powder. The powder obtained was characterized by XRD,TEM etc. The results of analysis showed that the ultrafine powder is of spinel phase, high purity, good dispersion.This process for preparing fine Magnesium aluminate spinel powder was very simple and inexpensive.The results of analysis showed that the ultrafine powder was of mullite phase, high purity, good dispersion, and the particle were homogeneous.


RSC Advances ◽  
2021 ◽  
Vol 11 (22) ◽  
pp. 13245-13255
Author(s):  
Mehdi Davoodi ◽  
Fatemeh Davar ◽  
Mohammad R. Rezayat ◽  
Mohammad T. Jafari ◽  
Mehdi Bazarganipour ◽  
...  

New nanocomposite of zeolitic imidazolate framework-67@magnesium aluminate spinel (ZIF-67@MgAl2O4) has been fabricated by a simple method at room temperature with different weight ratios.


2020 ◽  
Vol 1697 ◽  
pp. 012156
Author(s):  
V Bukina ◽  
O Dymshits ◽  
I Alekseeva ◽  
M Tsenter ◽  
S Zapalova ◽  
...  

Ifost ◽  
2013 ◽  
Author(s):  
Khasanov Oleg ◽  
Dvilis Edgar ◽  
Kachaev Artem ◽  
Khasanov Alexey ◽  
Polisadova Elena

2016 ◽  
Vol 100 (2) ◽  
pp. 554-562 ◽  
Author(s):  
Hidehiro Yoshida ◽  
Papiya Biswas ◽  
Roy Johnson ◽  
Mantravadi Krishna Mohan

2014 ◽  
Vol 633 ◽  
pp. 245-248
Author(s):  
Xin Lin ◽  
Yong Li ◽  
Yan Jing Li ◽  
Jun Jie Zhang ◽  
Chang He Gao ◽  
...  

Specimens were prepared using iron-rich magnesia (3~1 mm、≤1 mm) and high purity magnesia (≤0.088 mm) as the main starting materials, adding tabular alumina at different size (3~2、2~1、≤1 mm) and content:3%、6%、9%、12%、15% to discover the influence of tabular alumina on sample performance. Phase composition and microstructure were also analyzed. The results show that specimen with content of 6% of corundum possessed the best comprehensive performance:apparent porosity 17%, bulk density 2.95 g·cm-3, cold crushing strength 74 MPa, refractoriness under load 1700 °C, heat shock resistance of up to 18 times. The formations of magnesium aluminate spinel and hercynite solid solution were enhanced by Fe ion at high temperatures in the iron-rich magnesia-corundum system at the presence of iron oxides, which are able to largely dissolved in periclase.


2016 ◽  
Vol 42 (16) ◽  
pp. 18215-18222 ◽  
Author(s):  
Xiangong Deng ◽  
Junkai Wang ◽  
Jianghao Liu ◽  
Haijun Zhang ◽  
Lei Han ◽  
...  

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