ChemInform Abstract: OXAZOLONES, II. ACID HYDROLYSIS OF N-TERT-BUTYL-2-OXO-4,5-DIPHENYL-4-OXAZOLINE-3-CARBOXAMIDE

1976 ◽  
Vol 7 (29) ◽  
pp. no-no
Author(s):  
BENNO KRIEG ◽  
HANS LAUTENSCHLAEGER
Chemosphere ◽  
2020 ◽  
Vol 248 ◽  
pp. 125975
Author(s):  
Maxime Julien ◽  
Didier Gori ◽  
Patrick Höhener ◽  
Richard J. Robins ◽  
Gérald S. Remaud

1962 ◽  
Vol 41 (2) ◽  
pp. 234-246 ◽  
Author(s):  
H. J. van der Molen

ABSTRACT A procedure for the quantitative determination of 5β-pregnan-3α-ol-20-one in urine is described. After acid hydrolysis of the pregnanolone-conjugates in urine, the free steroids are extracted with toluene. Pregnanolone is isolated in a pure form as its acetate; after chromatographic separation of the free steroids on alumina, the fraction containing pregnanolone is acetylated and rechromatographed on alumina. Quantitative determination of the isolated pregnanolone-acetate is carried out with the aid of the infrared spectrum recorded by a micro KBr-wafermethod. The reliability of the method under various conditions is discussed under the headings, specificity, accuracy, precision and sensitivity. It is possible to determine 30–40 μg pregnanolone in a 24-hours urine portion with a precision of 25%.


Author(s):  
M. Alekseenko ◽  
V. Litvyak ◽  
A. Sysa ◽  
E. Hrabovska ◽  
O. Galenko

2012 ◽  
Vol 11 (12) ◽  
pp. 2313-2318
Author(s):  
Theodor Malutan ◽  
Adina Elena Panzariu

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