A Novel Method for the Synthesis of Formyl and Hydroxymethyl Derivatives of 4H-Pyran-4-one.

ChemInform ◽  
2003 ◽  
Vol 34 (2) ◽  
Author(s):  
M. Ghandi ◽  
Y. Bayat ◽  
R. Teimuri-mofrad
Keyword(s):  
Novel Method ◽  
Derivatives Of

TIME-TO-CONTACT INFORMATION ESTIMATION FOR MONOCULAR MOBILE ROBOTS

2008 ◽  
Vol 05 (03) ◽  
pp. 223-233 ◽  
Author(s):  
RONG LIU ◽  
MAX Q. H. MENG
Keyword(s):  
Mobile Robots ◽  
Optical Flow ◽  
Active Contour Model ◽  
Visual Navigation ◽  
Moving Object ◽  
Time To Contact ◽  
Temporal Derivative ◽  
Novel Method ◽  
Derivatives Of ◽  
Flow Experiments

Time-to-contact (TTC) provides vital information for obstacle avoidance and for the visual navigation of a robot. In this paper, we present a novel method to estimate the TTC information of a moving object for monocular mobile robots. In specific, the contour of the moving object is extracted first using an active contour model; then the height of the motion contour and its temporal derivative are evaluated to generate the desired TTC estimates. Compared with conventional techniques employing the first-order derivatives of optical flow, the proposed estimator is less prone to errors of optical flow. Experiments using real-world images are conducted and the results demonstrate that the developed method can successfully achieve TTC with an average relative error (ARVE) of 0.039 with a single calibrated camera.

scholarly journals New approach in the application of lignin for the synthesis of hybrid materials

2017 ◽  
Vol 89 (1) ◽  
pp. 161-171 ◽  
Author(s):  
Beata Podkościelna ◽  
Marta Goliszek ◽  
Olena Sevastyanova
Keyword(s):  
Suspension Polymerization ◽  
Nitrogen Adsorption ◽  
Experimental Protocol ◽  
New Approach ◽  
Surface Areas ◽  
Adsorption Data ◽  
Novel Method ◽  
Derivatives Of ◽  
Polymerization Method ◽  
Nitrogen Adsorption Data

AbstractIn this study, a novel method for the synthesis of hybrid, porous microspheres, including divinylbenzene (DVB), triethoxyvinylsilane (TEVS) and methacrylated lignin (L-Met), is presented. The methacrylic derivatives of kraft lignin were obtained by reaction with methacryloyl chloride according to a new experimental protocol. The course of the modification of lignin was confirmed by attenuated total reflectance (ATR-FTIR) and nuclear magnetic resonance (NMR) spectroscopy. The emulsion-suspension polymerization method was employed to obtain copolymers of DVD, TEVS and L-Met in spherical forms. The porous structures and morphologies of the obtained lignin-containing functionalized microspheres were investigated by low-temperature nitrogen adsorption data and scanning electron microscopy (SEM). The microspheres are demonstrated to be mesoporous materials with specific surface areas in the range of 430–520 m2/g. The effects of the lignin component on the porous structure, shape, swelling and thermal properties of the microspheres were evaluated.

scholarly journals The Synthesis of the Locating Substitution Derivatives of Chitosan by Click Reaction at the 6-Position of Chitin

2015 ◽  
Vol 2015 ◽  
pp. 1-9 ◽  
Author(s):  
Yu Chen ◽  
Yanchun Ye ◽  
Yanyan Jing ◽  
YuanYuan Gao ◽  
Yanwen Guo ◽  
...  
Keyword(s):  
Nucleophilic Substitution ◽  
High Efficiency ◽  
Click Reaction ◽  
Macrocyclic Compound ◽  
Optimum Conditions ◽  
Structures And Properties ◽  
Acetyl Group ◽  
Novel Method ◽  
Derivatives Of

A novel method to prepare the macrocyclic compound locating substitution derivatives of chitosan was investigated, by using cyclodextrin as the model of macrocyclic compound. The method combines the advantages of activated 6-OH of chitin and high efficiency of click reaction. Chitin C6-OHp-toluenesulfonate (CTN-6-OTs) was generated and subsequently transferred to chitin C6-N3via nucleophilic substitution. Afterwards,β-cyclodextrin was immobilized at 6-OH of chitin via click reaction to afford CTN-6-CD. Ultimately, CTS-6-CD was obtained by removing the acetyl group of chitin unit. The structures and properties of these products were characterized by FTIR, TG, and XRD, respectively. It was found that CTN-6-CD synthesized at the optimum conditions has an immobilized loading of1.6126×10-4 mol/g and that of the corresponding CTS-6-CD, generated by removal of the acetyl group, was1.6891×10-4 mol/g.

scholarly journals Cis-effects of heterochromatin on heterochromatic and euchromatic gene activity in Drosophila melanogaster.

Genetics ◽  
1995 ◽  
Vol 140 (3) ◽  
pp. 1033-1045
Author(s):  
M Howe ◽  
P Dimitri ◽  
M Berloco ◽  
B T Wakimoto
Keyword(s):  
Chromosomal Rearrangements ◽  
Position Effect ◽  
Position Effect Variegation ◽  
Regulatory Requirements ◽  
Molecular Studies ◽  
Effect Variegation ◽  
Novel Method ◽  
In Cis ◽  
Derivatives Of ◽  
Heterochromatic Genes

Abstract Chromosomal rearrangements that juxtapose heterochromatin and euchromatin can result in mosaic inactivation of heterochromatic and euchromatic genes. This phenomenon, position effect variegation (PEV), suggests that heterochromatic and euchromatic genes differ in their regulatory requirements. This report describes a novel method for mapping regions required for heterochromatic genes, and those that induce PEV of a euchromatic gene. P transposase mutagenesis was used to generate derivatives of a translocation that variegated for the light+ (lt+) gene and carried the euchromatic white+ (w+) gene on a transposon near the heterochromatin-euchromatin junction. Cytogenetic and genetic analyses of the derivatives showed that P mutagenesis resulted in deletions of several megabases of heterochromatin. Genetic and molecular studies showed that the derivatives shared a euchromatic breakpoint but differed in their heterochromatic breakpoint and their effects on seven heterochromatic genes and the w+ gene. Heterochromatic genes differed in their response to deletions. The lt+ gene was sensitive to the amount of heterochromatin at the breakpoint but the heterochromatic 40Fa gene was not. The severity of variegated w+ phenotype did not depend on the amount of heterochromatin in cis, but varied with local heterochromatic environment. These data are relevant for considering mechanisms of PEV of both heterochromatic and euchromatic genes.

A Novel Method for Load Bounds Identification for Uncertain Structures in Frequency Domain

2018 ◽  
Vol 15 (06) ◽  
pp. 1850051 ◽  
Author(s):  
Z. C. He ◽  
X. Y. Lin ◽  
Eric Li
Keyword(s):  
Least Squares ◽  
Frequency Domain ◽  
Interval Uncertainty ◽  
Uncertain Parameters ◽  
Interval Extension ◽  
Uncertain Structure ◽  
Novel Method ◽  
Uncertain Structures ◽  
Derivatives Of ◽  
Least Squares Approach

A novel method for load bounds identification for uncertain structures is proposed in the frequency domain. The uncertain parameters are assumed to locate in their intervals and only their bounds rather than their precise information are needed. To quantitatively describe the effect of the interval uncertainty on the load identification in the frequency ranges, the interval extension is then introduced in the frequency response function (FRF)-based least squares approach. Therefore, the load bounds are determined through the summation of the two separate parts including the midpoint part and the perturbed part of the load. The midpoint part is computed by using the Moore–Penrose pseudo-inversion and the perturbed part is transformed into the first derivatives of the midpoint load with respect to the uncertain parameters by applying the truncated total least squares (TTLS). Two numerical examples are investigated to validate that the proposed method is very effective to predict the load bounds for the uncertain structure in frequency domain.

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