Synthesis and characterization of a new phosphorus‐containing furan‐based epoxy curing agent as a flame retardant

2019 ◽  
Vol 43 (6) ◽  
pp. 717-724 ◽  
Author(s):  
Mai Toan ◽  
Ji‐Won Park ◽  
Hyung‐Jun Kim ◽  
Seunghan Shin
Keyword(s):  
Flame Retardant ◽  
Synthesis And Characterization ◽  
Curing Agent ◽  
Epoxy Curing ◽  
Phosphorus Containing

Synthesis and Characterization of a New Phosphorus-Containing Curing Agent PPDTA

2019 ◽  
Vol 953 ◽  
pp. 185-190
Author(s):  
Yong Li Peng ◽  
Ni An Zhuo ◽  
Can Zhang
Keyword(s):  
Infrared Spectroscopy ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Orthogonal Experiment ◽  
Molar Ratio ◽  
Synthesis And Characterization ◽  
Curing Agent ◽  
Phosphorus Containing ◽  
Three Factor

A new phosphorus-containing flame-retardant curing agent PPDTA was synthesized from phenylphosphonic dichloride (PPD) and 3-amino-1,2,4-triazole (TA) in tetrahydrofuran solvent to improve the flame retardancy of epoxy resin. The structure of the compound was analyzed and confirmed by infrared spectroscopy. The effects of reaction time, reaction temperature and ratio of reactants on yield were studied by using three-factor three-level orthogonal experiment. The results show that the yield of PPDTA can reach 86.4%, when the reaction time is 10h, reaction temperature is 70 °Cand the molar ratio of TA to PPD is 2.2:1.

Synthesis and characterization of a phosphorus-containing flame retardant with double bonds and its application in bismaleimide resins

RSC Advances ◽  
2015 ◽  
Vol 5 (123) ◽  
pp. 101480-101486 ◽  
Author(s):  
Song Li ◽  
Hongxia Yan ◽  
Shuyao Feng ◽  
Song Niu
Keyword(s):  
Mechanical Properties ◽  
Thermal Stability ◽  
Flame Retardant ◽  
Flame Retardancy ◽  
Synthesis And Characterization ◽  
Bismaleimide Resin ◽  
Phosphorus Containing ◽  
Reactive Phosphorus ◽  
Bismaleimide Resins

A novel reactive phosphorus-containing flame retardant was synthesized and used to modify bismaleimide resin. According to investigations, the modified bismaleimide resin has good mechanical properties, thermal stability and flame retardancy.

Preparation and characterization of flame retardant epoxy resins based on phosphorus-containing biphenyl-type phenolic resin

e-Polymers ◽  
2010 ◽  
Vol 10 (1) ◽  
Author(s):  
Jiapei Ding ◽  
Zhiqiang Tao ◽  
Lin Fan ◽  
Shiyong Yang
Keyword(s):  
Flame Retardant ◽  
Epoxy Resins ◽  
Phenolic Resin ◽  
Phosphorus Loading ◽  
Curing Agent ◽  
Good Thermal Stability ◽  
Phosphorus Containing ◽  
Strong Lewis Acid ◽  
Flame Retardant Properties

AbstractA phosphorus-containing biphenyl-type phenolic resin (PBP) was prepared by dehydration polycondensation of the DOPO-disubstituted 4,4’- biphenyldimethanol compound (BDCA-2DOPO) with phenol in the presence of strong Lewis acid , in which BDCA-2DOPO was prepared by the reaction of DOPO with 4,4'-biphenyldicarboxaldehyde. The PBP resin has been evaluated as the curing agent of o-cresol epoxy resins. Experimental results indicated that the PBPcured epoxy resins exhibited good thermal stability, high char yields at 700 oC and outstanding flame retardant properties. UL 94 V-0 classifications could be obtained when the phosphorus loading in the epoxy resin is higher than 1.8 wt%.

Synthesis and characterization of water-dispersed flame-retardant polyurethane resin using phosphorus-containing chain extender

2003 ◽  
Vol 91 (2) ◽  
pp. 1314-1321 ◽  
Author(s):  
Funda Çelebi ◽  
Osman Polat ◽  
Leyla Aras ◽  
Güngör Gündüz ◽  
Idris M. Akhmedov
Keyword(s):  
Flame Retardant ◽  
Chain Extender ◽  
Synthesis And Characterization ◽  
Polyurethane Resin ◽  
Phosphorus Containing

Synthesis and characterization of novel post-chain extension flame retardant waterborne polyurethane

RSC Advances ◽  
2015 ◽  
Vol 5 (118) ◽  
pp. 97710-97719 ◽  
Author(s):  
Gang Wu ◽  
Jinqing Li ◽  
Chunpeng Chai ◽  
Zhen Ge ◽  
Jialun Lin ◽  
...  
Keyword(s):  
Flame Retardant ◽  
Waterborne Polyurethane ◽  
Chain Extension ◽  
Synthesis And Characterization ◽  
Waterborne Polyurethanes ◽  
Phosphorus Containing

Flame-retardant waterborne polyurethanes with a phosphorus-containing flame retardant diamine (AWPUs) were synthesized and characterized by the method of post-chain extension technology.

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